C₂₁H₁₃ClF₃N₃O₂

Base Information

Chemical Name:C₂₁H₁₃ClF₃N₃O₂
CAS No.:1276035-64-3
Molecular Formula:C₂₁H₁₃ClF₃N₃O₂
Molecular Weight:431.801
Hs Code.:

C<sub>21</sub>H<sub>13</sub>ClF<sub>3</sub>N<sub>3</sub>O<sub>2</sub>

Synonyms:C₂₁H₁₃ClF₃N₃O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₁₃ClF₃N₃O₂

Chemical Property:

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Technology Process of C₂₁H₁₃ClF₃N₃O₂

There total 5 articles about C₂₁H₁₃ClF₃N₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1276040-20-0
C₁₃H₁₀F₃N₃O₂

: 104-88-1
4-chlorobenzaldehyde

: 122-51-0
orthoformic acid triethyl ester

: 1276035-64-3
C₂₁H₁₃ClF₃N₃O₂

Guidance literature:: C₁₃H₁₀F₃N₃O₂; 4-chlorobenzaldehyde; With sodium tris(acetoxy)borohydride; acetic acid; In 1,2-dichloro-ethane; at 20 ℃;

orthoformic acid triethyl ester; In 1,2-dichloro-ethane; at 80 ℃;

Reference yield:

: 59216-77-2
methyl 5-hydroxy-2-nitro-benzoate

: 1276035-64-3
C₂₁H₁₃ClF₃N₃O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / dimethyl sulfoxide / 100 °C

2.1: ammonia / methanol / 24 h / 100 °C / Sealed tube

3.1: hydrogen / Raney nickel / methanol / 24 h / 20 °C / 775.74 - 1034.32 Torr

4.1: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane / 20 °C

4.2: 80 °C

With ammonia; hydrogen; sodium tris(acetoxy)borohydride; potassium carbonate; acetic acid; Raney nickel; In methanol; dimethyl sulfoxide; 1,2-dichloro-ethane;

Reference yield:

: 1007374-52-8
C₁₄H₉F₃N₂O₅

: 1276035-64-3
C₂₁H₁₃ClF₃N₃O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonia / methanol / 24 h / 100 °C / Sealed tube

2.1: hydrogen / Raney nickel / methanol / 24 h / 20 °C / 775.74 - 1034.32 Torr

3.1: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane / 20 °C

3.2: 80 °C

With ammonia; hydrogen; sodium tris(acetoxy)borohydride; acetic acid; Raney nickel; In methanol; 1,2-dichloro-ethane;