C₃₃H₃₆ClNO₈S

Base Information

Chemical Name:C₃₃H₃₆ClNO₈S
CAS No.:951327-58-5
Molecular Formula:C₃₃H₃₆ClNO₈S
Molecular Weight:642.17
Hs Code.:

C<sub>33</sub>H<sub>36</sub>ClNO<sub>8</sub>S

Synonyms:C₃₃H₃₆ClNO₈S

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Chemical Property of C₃₃H₃₆ClNO₈S

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Technology Process of C₃₃H₃₆ClNO₈S

There total 13 articles about C₃₃H₃₆ClNO₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 951327-56-3
C₁₈H₂₆ClNO₅

: 218628-45-6
2-(3,4-Methylenedioxyphenyl)-2-(phenylthio)acetic acid

: 951327-58-5
C₃₃H₃₆ClNO₈S

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 30 ℃; for 3h;
DOI:10.1021/ol071344y

Reference yield:

: 951327-39-2
C₁₈H₂₅ClO₇

: 951327-58-5
C₃₃H₃₆ClNO₈S

Guidance literature:: Multi-step reaction with 8 steps

1: 66 percent / triiodoimidazole; imidazole; PPh₃ / toluene / 5 h / Heating

2: 84 percent / n-Bu₃SnH; Et₃B; O₂ / toluene; hexane / 2 h / 18 °C

3: 98 percent / DDQ / CH₂Cl₂; H₂O / 20 h / 18 °C

4: 75 percent / diphenylphosphoryl azide; DEAD; PPh₃ / CH₂Cl₂ / 18 h / 18 °C

5: 98 percent / PPh₃; H₂O / tetrahydrofuran / 20 h / 65 °C

6: benzene / 16 h / Heating

7: sodium cyanoborohydride / methanol / 1 h / 18 °C

8: 74 percent / EDCI; HOBt; i-Pr₂NEt / dimethylformamide / 3 h / 30 °C

With 1H-imidazole; triethyl borane; tri-iodoimidazole; diphenylphosphoranyl azide; water; oxygen; tri-n-butyl-tin hydride; sodium cyanoborohydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; diethylazodicarboxylate; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene; benzene; 4: Mitsunobu reaction / 5: Staudinger reaction;
DOI:10.1021/ol071344y

Reference yield:

: 951327-37-0
C₁₈H₂₃ClO₇

: 951327-58-5
C₃₃H₃₆ClNO₈S

Guidance literature:: Multi-step reaction with 9 steps

1: 60 percent / DIBAL-H / toluene / 7.5 h / -30 °C

2: 66 percent / triiodoimidazole; imidazole; PPh₃ / toluene / 5 h / Heating

3: 84 percent / n-Bu₃SnH; Et₃B; O₂ / toluene; hexane / 2 h / 18 °C

4: 98 percent / DDQ / CH₂Cl₂; H₂O / 20 h / 18 °C

5: 75 percent / diphenylphosphoryl azide; DEAD; PPh₃ / CH₂Cl₂ / 18 h / 18 °C

6: 98 percent / PPh₃; H₂O / tetrahydrofuran / 20 h / 65 °C

7: benzene / 16 h / Heating

8: sodium cyanoborohydride / methanol / 1 h / 18 °C

9: 74 percent / EDCI; HOBt; i-Pr₂NEt / dimethylformamide / 3 h / 30 °C

With 1H-imidazole; triethyl borane; tri-iodoimidazole; diphenylphosphoranyl azide; water; oxygen; tri-n-butyl-tin hydride; diisobutylaluminium hydride; sodium cyanoborohydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; diethylazodicarboxylate; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene; benzene; 5: Mitsunobu reaction / 6: Staudinger reaction;
DOI:10.1021/ol071344y