N^4a-<1-(4-biphenylyl)-1-methylethoxycarbonyl>-L-glutamine pentafluorophenyl ester

Base Information

• Chemical Name: N^4a-<1-(4-biphenylyl)-1-methylethoxycarbonyl>-L-glutamine pentafluorophenyl ester
• CAS No.: 75695-22-6
• Molecular Formula: C₂₇H₂₃F₅N₂O₅
• Molecular Weight: 550.482

Synonyms:N^4a-<1-(4-biphenylyl)-1-methylethoxycarbonyl>-L-glutamine pentafluorophenyl ester

Chemical Property of N^4a-<1-(4-biphenylyl)-1-methylethoxycarbonyl>-L-glutamine pentafluorophenyl ester

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Technology Process of N^4a-<1-(4-biphenylyl)-1-methylethoxycarbonyl>-L-glutamine pentafluorophenyl ester

There total 1 articles about N^4a-<1-(4-biphenylyl)-1-methylethoxycarbonyl>-L-glutamine pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2,3,4,5,6-pentafluorophenol (771-61-9) + N4a-<1-(4-biphenylyl)-1-methylethoxycarbonyl>-L-glutamine (25692-86-8) → N4a-<1-(4-biphenylyl)-1-methylethoxycarbonyl>-L-glutamine pentafluorophenyl ester (75695-22-6)

Guidance literature:

With dicyclohexyl-carbodiimide; In ethyl acetate; at 0 ℃; for 1h;

Reference yield: 81.0%

S-trityl-L-cysteine (2799-07-7) + N4a-<1-(4-biphenylyl)-1-methylethoxycarbonyl>-L-glutamine pentafluorophenyl ester (75695-22-6) → N4a-<1-(4-biphenylyl)-1-methylethoxycarbonyl>-L-glutaminyl-S-trityl-L-cysteine

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 0 ℃; for 1h;

Reference yield:

N4a-<1-(4-biphenylyl)-1-methylethoxycarbonyl>-L-glutamine pentafluorophenyl ester (75695-22-6) → N4a-<1-(4-biphenylyl)-1-methylethoxycarbonyl>-L-glutaminyl-S-trityl-L-cysteine pentafluorophenyl ester

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / triethylamine / dimethylformamide / 1 h / 0 °C

2: DCC / ethyl acetate / 1) 1h, 0 deg C, 2) 30 min, 20 deg C

With triethylamine; dicyclohexyl-carbodiimide; In ethyl acetate; N,N-dimethyl-formamide;

upstream raw materials:

2,3,4,5,6-pentafluorophenol

N^4a-<1-(4-biphenylyl)-1-methylethoxycarbonyl>-L-glutamine

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