N³-(N'-(4-trimethylammonium-3-trifluoromethyl-benzoyl))-3-amino-propyl-thymidine triflate salt

Base Information

• Chemical Name: N³-(N'-(4-trimethylammonium-3-trifluoromethyl-benzoyl))-3-amino-propyl-thymidine triflate salt
• CAS No.: 1021905-37-2
• Molecular Formula: CF₃O₃S*C₂₄H₃₂F₃N₄O₆
• Molecular Weight: 678.607

Synonyms:N³-(N'-(4-trimethylammonium-3-trifluoromethyl-benzoyl))-3-amino-propyl-thymidine triflate salt

Chemical Property of N³-(N'-(4-trimethylammonium-3-trifluoromethyl-benzoyl))-3-amino-propyl-thymidine triflate salt

Chemical Property:

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Technology Process of N³-(N'-(4-trimethylammonium-3-trifluoromethyl-benzoyl))-3-amino-propyl-thymidine triflate salt

There total 1 articles about N³-(N'-(4-trimethylammonium-3-trifluoromethyl-benzoyl))-3-amino-propyl-thymidine triflate salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

trifluoro-methanesulfonate(4-carboxy-2-trifluoromethyl-phenyl)-trimethylammonium + 3-(3-Amino-propyl)-1-[(2R,4S,5R)-4-(1-methoxy-cyclohexyloxy)-5-(1-methoxy-cyclohexyloxymethyl)-tetrahydro-furan-2-yl]-5-methyl-1H-pyrimidine-2,4-dione (1021905-52-1) → N3-(N'-(4-trimethylammonium-3-trifluoromethyl-benzoyl))-3-amino-propyl-thymidine triflate salt (1021905-37-2)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide; for 8h;

Reference yield:

N3-(N'-(4-trimethylammonium-3-trifluoromethyl-benzoyl))-3-amino-propyl-thymidine triflate salt (1021905-37-2) → N3-(3-(N-(4-[18F]-fluoro-3-trifluoromethyl-benzoyl))aminopropyl)-thymidine (1021905-38-3)

Guidance literature:

N³-(N'-(4-trimethylammonium-3-trifluoromethyl-benzoyl))-3-amino-propyl-thymidine triflate salt; With [¹⁸F]fluoride; potassium carbonate; [2.2.2]cryptande; In acetonitrile; at 20 - 70 ℃; for 0.25h; Radiochemical reaction;

With hydrogenchloride; In water; acetonitrile; at 20 - 105 ℃; for 0.0833333h; Radiochemical reaction; Acidic aqueous solution;

upstream raw materials:

3-(3-Amino-propyl)-1-[(2R,4S,5R)-4-(1-methoxy-cyclohexyloxy)-5-(1-methoxy-cyclohexyloxymethyl)-tetrahydro-furan-2-yl]-5-methyl-1H-pyrimidine-2,4-dione

Downstream raw materials:

N³-(3-(N-(4-[¹⁸F]-fluoro-3-trifluoromethyl-benzoyl))aminopropyl)-thymidine

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