tris(tetraethylammonium) hexakis(p-methylphenylthiolato)hexakis(μ3-sulfido)hexaferrate(3II,3III)

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Chemical Name:tris(tetraethylammonium) hexakis(p-methylphenylthiolato)hexakis(μ3-sulfido)hexaferrate(3II,3III)
CAS No.:94499-98-6
Molecular Formula:3C₈H₂₀N*C₄₂H₄₂Fe₆S₁₂
Molecular Weight:1657.43
Hs Code.:

Synonyms:tris(tetraethylammonium) hexakis(p-methylphenylthiolato)hexakis(μ3-sulfido)hexaferrate(3II,3III)

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Chemical Property of tris(tetraethylammonium) hexakis(p-methylphenylthiolato)hexakis(μ3-sulfido)hexaferrate(3II,3III)

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Technology Process of tris(tetraethylammonium) hexakis(p-methylphenylthiolato)hexakis(μ3-sulfido)hexaferrate(3II,3III)

There total 1 articles about tris(tetraethylammonium) hexakis(p-methylphenylthiolato)hexakis(μ3-sulfido)hexaferrate(3II,3III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 94499-90-8
tris(tetraethylammonium) hexachlorohexakis(μ3-sulfido)hexaferrate(3II,3III)*acetonitrile

: 10486-08-5
sodium p-thiocresolate

: 94499-98-6
tris(tetraethylammonium) hexakis(p-methylphenylthiolato)hexakis(μ3-sulfido)hexaferrate(3II,3III)

Guidance literature:: In acetonitrile; byproducts: NaCl; (NEt4)3Fe6S6Cl6 and NaSC6H4-pMe are added to MeCN, resulting soln. is stirred for 5 min (under N2); soln. is filtered to remove NaCl, to the filtrate is added Et2O, soln. is stood overnight at -20°C, ppt. is filtered (crude product);
DOI:10.1021/ja00290a034