(3aS,8aR)-8-benzyl-1-methyl-3a-(3-methylbut-2-enyl)-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole

Base Information

Chemical Name:(3aS,8aR)-8-benzyl-1-methyl-3a-(3-methylbut-2-enyl)-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole
CAS No.:1380585-92-1
Molecular Formula:C₂₃H₂₈N₂
Molecular Weight:332.489
Hs Code.:

Synonyms:(3aS,8aR)-8-benzyl-1-methyl-3a-(3-methylbut-2-enyl)-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole

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Chemical Property of (3aS,8aR)-8-benzyl-1-methyl-3a-(3-methylbut-2-enyl)-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole

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Technology Process of (3aS,8aR)-8-benzyl-1-methyl-3a-(3-methylbut-2-enyl)-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole

There total 25 articles about (3aS,8aR)-8-benzyl-1-methyl-3a-(3-methylbut-2-enyl)-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: C₂₃H₂₆N₂O

: 1380585-92-1
(3aS,8aR)-8-benzyl-1-methyl-3a-(3-methylbut-2-enyl)-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole

Guidance literature:: With alane-N,N-dimethylethylamine complex; In tetrahydrofuran; toluene; at 20 ℃; for 0.116667h;
DOI:10.1016/j.tet.2013.08.057

Reference yield: 86.0%

: 1380585-91-0
(S)-1-benzyl-3-(2-(methylamino)ethyl)-3-(3-methylbut-2-enyl)indolin-2-one

: 1380585-92-1
(3aS,8aR)-8-benzyl-1-methyl-3a-(3-methylbut-2-enyl)-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; at 0 - 75 ℃; for 13.5h; Inert atmosphere;
DOI:10.1021/ol3012056

Reference yield:

: (S)-N-(2-(1-benzyl-3-(3-methylbut-2-enyl)-2-oxoindolin-3-yl)ethyl)-N,2-dimethylpropane-2-sulfinamide

: 1380585-92-1
(3aS,8aR)-8-benzyl-1-methyl-3a-(3-methylbut-2-enyl)-1,2,3,3a,8,8a-hexahydropyrrolo[2,3-b]indole

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / 1,4-dioxane; methanol; water / 3 h / 20 °C / Inert atmosphere

2: diisobutylaluminium hydride / tetrahydrofuran / 13.5 h / 0 - 75 °C / Inert atmosphere

With hydrogenchloride; diisobutylaluminium hydride; In tetrahydrofuran; 1,4-dioxane; methanol; water;
DOI:10.1021/ol3012056