Technology Process of C17H16ClFN2O6
There total 13 articles about C17H16ClFN2O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetra(n-butyl)ammonium hydroxide; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid;
In
dichloromethane;
for 12h;
pH=4;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
2: triethylamine tris(hydrogen fluoride); N-iodo-succinimide / acetonitrile / 5 h / 20 °C / Inert atmosphere
3: dmap; triethylamine / dichloromethane / 12 h / 20 °C
4: 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; tetra(n-butyl)ammonium hydroxide / dichloromethane / 12 h / pH 4
With
dmap; N-iodo-succinimide; tetra(n-butyl)ammonium hydroxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine tris(hydrogen fluoride); triethylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: ammonia / methanol / 12 h / 20 °C
2: triphenylphosphine; 1H-imidazole; pyridine; iodine / tetrahydrofuran / 0 - 20 °C
3: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
4: triethylamine tris(hydrogen fluoride); N-iodo-succinimide / acetonitrile / 5 h / 20 °C / Inert atmosphere
5: dmap; triethylamine / dichloromethane / 12 h / 20 °C
6: 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; tetra(n-butyl)ammonium hydroxide / dichloromethane / 12 h / pH 4
With
pyridine; 1H-imidazole; dmap; N-iodo-succinimide; tetra(n-butyl)ammonium hydroxide; ammonia; iodine; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine tris(hydrogen fluoride); triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; trifluoroacetic acid;
In
tetrahydrofuran; methanol; dichloromethane; acetonitrile;