4-hydroxy-4-methoxycarbonyl-3,5-diphenyl-2-(3-methylpyridin-2-ylimino)thiazolidine

Base Information

• Chemical Name: 4-hydroxy-4-methoxycarbonyl-3,5-diphenyl-2-(3-methylpyridin-2-ylimino)thiazolidine
• CAS No.: 1109168-41-3
• Molecular Formula: C₂₃H₂₁N₃O₃S
• Molecular Weight: 419.504

Synonyms:4-hydroxy-4-methoxycarbonyl-3,5-diphenyl-2-(3-methylpyridin-2-ylimino)thiazolidine

Chemical Property of 4-hydroxy-4-methoxycarbonyl-3,5-diphenyl-2-(3-methylpyridin-2-ylimino)thiazolidine

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Technology Process of 4-hydroxy-4-methoxycarbonyl-3,5-diphenyl-2-(3-methylpyridin-2-ylimino)thiazolidine

There total 2 articles about 4-hydroxy-4-methoxycarbonyl-3,5-diphenyl-2-(3-methylpyridin-2-ylimino)thiazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(3-methylpyridin-2-yl)-N'-phenyl-thiourea (53385-83-4) + methyl 3-phenyl-3-chloro-2-ketopropionate (32803-73-9) → 4-hydroxy-4-methoxycarbonyl-3,5-diphenyl-2-(3-methylpyridin-2-ylimino)thiazolidine (1109168-41-3) + 4-hydroxy-4-methoxycarbonyl-5-phenyl-2-phenylimino-3-(3-methylpyridin-2-yl)thiazolidine (1109168-25-3)

Guidance literature:

With sodium acetate; In dichloromethane; at -20 - 20 ℃; for 5h;

DOI:10.1016/j.tet.2012.06.084

Reference yield:

methyl 3-phenyl-3-chloro-2-ketopropionate (32803-73-9) + N-(3-methyl-2-pyridyl)-N'-(phenyl)-thiourea (31979-23-4) → 4-hydroxy-4-methoxycarbonyl-3,5-diphenyl-2-(3-methylpyridin-2-ylimino)thiazolidine (1109168-41-3) + 4-hydroxy-4-methoxycarbonyl-5-phenyl-2-phenylimino-3-(3-methylpyridin-2-yl)thiazolidine (1109168-25-3)

Guidance literature:

In dichloromethane; for 5h; Title compound not separated from byproducts.;

DOI:10.1007/s11172-007-0365-9

Reference yield: 80.0%

4-hydroxy-4-methoxycarbonyl-3,5-diphenyl-2-(3-methylpyridin-2-ylimino)thiazolidine (1109168-41-3) + 1,2-diamino-benzene (95-54-5) → 3-phenyl-1-(3-methylpyridin-2-yl)iminothiazolo[3,4-a]quinoxalin-4(5H)-one

Guidance literature:

With acetic acid; for 2h; Reflux;

DOI:10.1016/j.tet.2012.06.084

upstream raw materials:

methyl 3-phenyl-3-chloro-2-ketopropionate

N-(3-methyl-2-pyridyl)-N'-(phenyl)-thiourea

N-(3-methylpyridin-2-yl)-N'-phenyl-thiourea

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