5,5'-(2,2-bis((3,5-dicarboxyphenoxy)methyl)propane-1,3-diyl)bis(oxy)diisophthalic acid

Base Information

Chemical Name:5,5'-(2,2-bis((3,5-dicarboxyphenoxy)methyl)propane-1,3-diyl)bis(oxy)diisophthalic acid
CAS No.:1315269-33-0
Molecular Formula:C₃₇H₂₈O₂₀
Molecular Weight:792.617
Hs Code.:

Synonyms:5,5'-(2,2-bis((3,5-dicarboxyphenoxy)methyl)propane-1,3-diyl)bis(oxy)diisophthalic acid

Suppliers and Price of 5,5'-(2,2-bis((3,5-dicarboxyphenoxy)methyl)propane-1,3-diyl)bis(oxy)diisophthalic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5,5'-(2,2-bis((3,5-dicarboxyphenoxy)methyl)propane-1,3-diyl)bis(oxy)diisophthalic acid

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 5,5'-(2,2-bis((3,5-dicarboxyphenoxy)methyl)propane-1,3-diyl)bis(oxy)diisophthalic acid

There total 1 articles about 5,5'-(2,2-bis((3,5-dicarboxyphenoxy)methyl)propane-1,3-diyl)bis(oxy)diisophthalic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 3229-00-3
pentaerythritol tetrabromide

: 13036-02-7
Dimethyl 5-hydroxyisophthalate

: 1315269-33-0
5,5'-(2,2-bis((3,5-dicarboxyphenoxy)methyl)propane-1,3-diyl)bis(oxy)diisophthalic acid

Guidance literature:: pentaerythritol tetrabromide; Dimethyl 5-hydroxyisophthalate; With potassium carbonate; In N,N-dimethyl-formamide; at 20 - 100 ℃; for 72.33h;

With potassium hydroxide; In ethanol; water; for 6h; Reflux;
DOI:10.1016/j.poly.2016.10.050

Reference yield: 86.0%

: zinc(II) nitrate hexahydrate

: 758-96-3
N,N-dimethyl-propanamide

: 1315269-33-0
5,5'-(2,2-bis((3,5-dicarboxyphenoxy)methyl)propane-1,3-diyl)bis(oxy)diisophthalic acid

: Zn₁₀O₂(5,5'-(2,2-bis((3,5-dicarboxyphenoxy)methyl)propane-1,3-diyl)bis(oxy)diisophthalate)2(N,N-dimethylpropionamide)2(H₂O)9

Guidance literature:: In further solvent(s); High Pressure; mixt. Zn(NO3)2*6H2O and ligand were dissolved in DMP and heated in Teflon-lined stainless steel container at 85°C for 72 h; ppt. was washed with DEA; elem. anal.;
DOI:10.1021/ic202635a

Reference yield: 82.0%

: zinc(II) nitrate hexahydrate

: 1315269-33-0
5,5'-(2,2-bis((3,5-dicarboxyphenoxy)methyl)propane-1,3-diyl)bis(oxy)diisophthalic acid

: [Zn₁₆(5,5'-(2,2-bis((3,5-dicarboxyphenoxy)methyl)propane-1,3-diyl)bis(oxy)diisophthalate)3(H₂O)16](NO₃)8

Guidance literature:: In further solvent(s); High Pressure; mixt. Zn(NO3)2*6H2O and ligand were dissolved in N,N-diethylpropionamideand heated in Teflon-lined stainless steel container at 85°C for 72 h; ppt. was washed with DEP; elem. anal.;
DOI:10.1021/ic202635a