2-methyl-acrylic acid 3-[2-(diethoxy-phosphoryl)-4-(1-{3-(diethoxy-phosphoryl)-4-[2-hydroxy-3-(2-methyl-acryloyloxy)-propoxy]-phenyl}-1-methyl-ethyl)-phenoxy]-2-hydroxy-propyl ester

Base Information

Chemical Name:2-methyl-acrylic acid 3-[2-(diethoxy-phosphoryl)-4-(1-{3-(diethoxy-phosphoryl)-4-[2-hydroxy-3-(2-methyl-acryloyloxy)-propoxy]-phenyl}-1-methyl-ethyl)-phenoxy]-2-hydroxy-propyl ester
CAS No.:270251-02-0
Molecular Formula:C₃₇H₅₄O₁₄P₂
Molecular Weight:784.775
Hs Code.:

2-methyl-acrylic acid 3-[2-(diethoxy-phosphoryl)-4-(1-{3-(diethoxy-phosphoryl)-4-[2-hydroxy-3-(2-methyl-acryloyloxy)-propoxy]-phenyl}-1-methyl-ethyl)-phenoxy]-2-hydroxy-propyl ester

Synonyms:2-methyl-acrylic acid 3-[2-(diethoxy-phosphoryl)-4-(1-{3-(diethoxy-phosphoryl)-4-[2-hydroxy-3-(2-methyl-acryloyloxy)-propoxy]-phenyl}-1-methyl-ethyl)-phenoxy]-2-hydroxy-propyl ester

Suppliers and Price of 2-methyl-acrylic acid 3-[2-(diethoxy-phosphoryl)-4-(1-{3-(diethoxy-phosphoryl)-4-[2-hydroxy-3-(2-methyl-acryloyloxy)-propoxy]-phenyl}-1-methyl-ethyl)-phenoxy]-2-hydroxy-propyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-methyl-acrylic acid 3-[2-(diethoxy-phosphoryl)-4-(1-{3-(diethoxy-phosphoryl)-4-[2-hydroxy-3-(2-methyl-acryloyloxy)-propoxy]-phenyl}-1-methyl-ethyl)-phenoxy]-2-hydroxy-propyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2-methyl-acrylic acid 3-[2-(diethoxy-phosphoryl)-4-(1-{3-(diethoxy-phosphoryl)-4-[2-hydroxy-3-(2-methyl-acryloyloxy)-propoxy]-phenyl}-1-methyl-ethyl)-phenoxy]-2-hydroxy-propyl ester

There total 5 articles about 2-methyl-acrylic acid 3-[2-(diethoxy-phosphoryl)-4-(1-{3-(diethoxy-phosphoryl)-4-[2-hydroxy-3-(2-methyl-acryloyloxy)-propoxy]-phenyl}-1-methyl-ethyl)-phenoxy]-2-hydroxy-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 760-93-0
methacryloyl anhydride

: 270251-01-9
C₂₉H₄₆O₁₂P₂

: 270251-02-0
2-methyl-acrylic acid 3-[2-(diethoxy-phosphoryl)-4-(1-{3-(diethoxy-phosphoryl)-4-[2-hydroxy-3-(2-methyl-acryloyloxy)-propoxy]-phenyl}-1-methyl-ethyl)-phenoxy]-2-hydroxy-propyl ester

Guidance literature:: With pyridine; dmap; at 20 ℃; for 18h;
DOI:10.1039/a909877a

Reference yield: 29.0%

: 270251-01-9
C₂₉H₄₆O₁₂P₂

: 920-46-7,26937-45-1
Methacryloyl chloride

: 270251-02-0
2-methyl-acrylic acid 3-[2-(diethoxy-phosphoryl)-4-(1-{3-(diethoxy-phosphoryl)-4-[2-hydroxy-3-(2-methyl-acryloyloxy)-propoxy]-phenyl}-1-methyl-ethyl)-phenoxy]-2-hydroxy-propyl ester

Guidance literature:: With pyridine;
DOI:10.1039/a909877a

Reference yield:

: 80-05-7
BPA

: 270251-02-0
2-methyl-acrylic acid 3-[2-(diethoxy-phosphoryl)-4-(1-{3-(diethoxy-phosphoryl)-4-[2-hydroxy-3-(2-methyl-acryloyloxy)-propoxy]-phenyl}-1-methyl-ethyl)-phenoxy]-2-hydroxy-propyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / Et₃N; CCl₄ / 30 h / 20 °C

2: 86 percent / LDA / tetrahydrofuran / 4 h / -78 - 20 °C

3: 50 percent / Et₃N / 3 h / Heating

4: 50 percent / pyridine; DMAP / 18 h / 20 °C

With pyridine; tetrachloromethane; dmap; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; 1: Addition / 2: Rearrangement / 3: Ring cleavage / 4: Esterification;
DOI:10.1039/a909877a