Technology Process of C14H16O5S
There total 6 articles about C14H16O5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine; methanesulfonyl chloride;
at 0 - 4 ℃;
for 16h;
diastereoselective reaction;
Inert atmosphere;
DOI:10.1002/ejoc.201300935
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylamine / dichloromethane / 16 h / 0 °C / Inert atmosphere
2: dmap; pyridine / 24 h / 0 - 20 °C / Inert atmosphere
3: sodium hydroxide / 1,4-dioxane / 1 h / Inert atmosphere; Reflux
4: magnesium bis(monoperoxyphthalate)hexahydrate / methanol / 6 h / 20 °C / Inert atmosphere
5: pyridine; methanesulfonyl chloride / 16 h / 0 - 4 °C / Inert atmosphere
With
pyridine; dmap; magnesium bis(monoperoxyphthalate)hexahydrate; methanesulfonyl chloride; triethylamine; sodium hydroxide;
In
1,4-dioxane; methanol; dichloromethane;
DOI:10.1002/ejoc.201300935
- Guidance literature:
-
Multi-step reaction with 6 steps
1: acetyl chloride / methanol / 2 h / 0 - 20 °C / Inert atmosphere
2: triethylamine / dichloromethane / 16 h / 0 °C / Inert atmosphere
3: dmap; pyridine / 24 h / 0 - 20 °C / Inert atmosphere
4: sodium hydroxide / 1,4-dioxane / 1 h / Inert atmosphere; Reflux
5: magnesium bis(monoperoxyphthalate)hexahydrate / methanol / 6 h / 20 °C / Inert atmosphere
6: pyridine; methanesulfonyl chloride / 16 h / 0 - 4 °C / Inert atmosphere
With
pyridine; dmap; magnesium bis(monoperoxyphthalate)hexahydrate; methanesulfonyl chloride; triethylamine; acetyl chloride; sodium hydroxide;
In
1,4-dioxane; methanol; dichloromethane;
DOI:10.1002/ejoc.201300935
