O,O'-(1,1'-dinaphthyl-2,2'-diyl)-N-(1-benzyloxyallyl)-N-but-3-enylamido phosphate

Base Information

Chemical Name:O,O'-(1,1'-dinaphthyl-2,2'-diyl)-N-(1-benzyloxyallyl)-N-but-3-enylamido phosphate
CAS No.:741252-63-1
Molecular Formula:C₃₄H₃₀NO₄P
Molecular Weight:547.59
Hs Code.:

Synonyms:O,O'-(1,1'-dinaphthyl-2,2'-diyl)-N-(1-benzyloxyallyl)-N-but-3-enylamido phosphate

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Chemical Property of O,O'-(1,1'-dinaphthyl-2,2'-diyl)-N-(1-benzyloxyallyl)-N-but-3-enylamido phosphate

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Technology Process of O,O'-(1,1'-dinaphthyl-2,2'-diyl)-N-(1-benzyloxyallyl)-N-but-3-enylamido phosphate

There total 3 articles about O,O'-(1,1'-dinaphthyl-2,2'-diyl)-N-(1-benzyloxyallyl)-N-but-3-enylamido phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 67515-49-5
1-benzyloxyallene

: 741252-61-9
O,O'-(1,1'-dinaphthyl-2,2'-diyl)-N-but-3-en-1-ylamidophosphate

: 741252-63-1
O,O'-(1,1'-dinaphthyl-2,2'-diyl)-N-(1-benzyloxyallyl)-N-but-3-enylamido phosphate

Guidance literature:: With 1,3-bis-(diphenylphosphino)propane; triethylamine; palladium diacetate; In acetonitrile; at 60 ℃; for 16h;

Reference yield:

: 124583-86-4,124583-87-5,124648-60-8
(+/-)-1,1'-Binaphthyl-2,2'-diyl phosphorochloridate

: 741252-63-1
O,O'-(1,1'-dinaphthyl-2,2'-diyl)-N-(1-benzyloxyallyl)-N-but-3-enylamido phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.42 g / CH₂Cl₂ / 17 h / 0 - 20 °C

2: 70 percent / Et₃N; dppp / Pd(OAc)2 / acetonitrile / 16 h / 60 °C

With 1,3-bis-(diphenylphosphino)propane; triethylamine; palladium diacetate; In dichloromethane; acetonitrile;

Reference yield:

: 602-09-5
1,1'-bi-2-naphthol

: 741252-63-1
O,O'-(1,1'-dinaphthyl-2,2'-diyl)-N-(1-benzyloxyallyl)-N-but-3-enylamido phosphate

Guidance literature:: Multi-step reaction with 3 steps

1: POCl₃; Et₃N / CH₂Cl₂ / 0.5 h

2: 1.42 g / CH₂Cl₂ / 17 h / 0 - 20 °C

3: 70 percent / Et₃N; dppp / Pd(OAc)2 / acetonitrile / 16 h / 60 °C

With 1,3-bis-(diphenylphosphino)propane; triethylamine; trichlorophosphate; palladium diacetate; In dichloromethane; acetonitrile;