4-O-Acetyl-3-(3-O-benzyl-2,6-dideoxy-4-O-methyl-α-D-lyxo-pyranosyl)-2,6-dideoxy-β-D-lyxo-pyranose

Base Information

Chemical Name:4-O-Acetyl-3-(3-O-benzyl-2,6-dideoxy-4-O-methyl-α-D-lyxo-pyranosyl)-2,6-dideoxy-β-D-lyxo-pyranose
CAS No.:131013-42-8
Molecular Formula:C₂₂H₃₂O₈
Molecular Weight:424.491
Hs Code.:

Synonyms:4-O-Acetyl-3-(3-O-benzyl-2,6-dideoxy-4-O-methyl-α-D-lyxo-pyranosyl)-2,6-dideoxy-β-D-lyxo-pyranose

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Chemical Property of 4-O-Acetyl-3-(3-O-benzyl-2,6-dideoxy-4-O-methyl-α-D-lyxo-pyranosyl)-2,6-dideoxy-β-D-lyxo-pyranose

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Technology Process of 4-O-Acetyl-3-(3-O-benzyl-2,6-dideoxy-4-O-methyl-α-D-lyxo-pyranosyl)-2,6-dideoxy-β-D-lyxo-pyranose

There total 12 articles about 4-O-Acetyl-3-(3-O-benzyl-2,6-dideoxy-4-O-methyl-α-D-lyxo-pyranosyl)-2,6-dideoxy-β-D-lyxo-pyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 131013-35-9,131013-46-2
tert-Butyldimethylsilyl 4-O-Acetyl-3-O-benzyl-2,6-dideoxy-D-lyxo-pyranoside

: 131013-42-8
4-O-Acetyl-3-(3-O-benzyl-2,6-dideoxy-4-O-methyl-α-D-lyxo-pyranosyl)-2,6-dideoxy-β-D-lyxo-pyranose

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 10percent Pd/C / ethanol / 48 h / 23 °C / 760 Torr

2: NBS / acetonitrile; tetrahydrofuran / 1) -42 deg C, 50 min, 2) 23 deg C, 10 min

3: Et₃NHF / acetonitrile / 2.5 h / 70 °C

With N-Bromosuccinimide; hydrogen; triethylamine hydrofluoride; palladium on activated charcoal; In tetrahydrofuran; ethanol; acetonitrile;
DOI:10.1021/jo00004a054

Reference yield:

: 131013-40-6
tert-Butyldimethylsilyl 4-O-Acetyl-3-(3-O-benzyl-2,6-dideoxy-4-O-methyl-α-D-lyxo-pyranosyl)-2,6-dideoxy-β-D-lyxo-pyranoside

: 131013-42-8
4-O-Acetyl-3-(3-O-benzyl-2,6-dideoxy-4-O-methyl-α-D-lyxo-pyranosyl)-2,6-dideoxy-β-D-lyxo-pyranose

: 131041-37-7
4-O-Acetyl-3-(3-O-benzyl-2,6-dideoxy-4-O-methyl-α-D-lyxo-pyranosyl)-2,6-dideoxy-α-D-lyxo-pyranose

Guidance literature:: With triethylamine hydrofluoride; In acetonitrile; at 70 ℃; for 2.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00004a054

Reference yield:

: 131013-38-2
tert-Butyldimethylsilyl 4-O-Acetyl-3-(3-O-benzyl-2,6-dideoxy-4-O-methyl-α-D-lyxo-pyranosyl)-2,6-dideoxy-α-D-lyxo-pyranoside

: 131013-42-8
4-O-Acetyl-3-(3-O-benzyl-2,6-dideoxy-4-O-methyl-α-D-lyxo-pyranosyl)-2,6-dideoxy-β-D-lyxo-pyranose

: 131041-37-7
4-O-Acetyl-3-(3-O-benzyl-2,6-dideoxy-4-O-methyl-α-D-lyxo-pyranosyl)-2,6-dideoxy-α-D-lyxo-pyranose

Guidance literature:: With triethylamine hydrofluoride; In acetonitrile; at 70 ℃; for 2.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00004a054