4-nitrophenyl 2-acetamido-6-O-tert-butylphenylsilyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:4-nitrophenyl 2-acetamido-6-O-tert-butylphenylsilyl-2-deoxy-β-D-glucopyranoside
CAS No.:467448-46-0
Molecular Formula:C₃₀H₃₆N₂O₈Si
Molecular Weight:580.71
Hs Code.:

Synonyms:4-nitrophenyl 2-acetamido-6-O-tert-butylphenylsilyl-2-deoxy-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-nitrophenyl 2-acetamido-6-O-tert-butylphenylsilyl-2-deoxy-β-D-glucopyranoside

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Technology Process of 4-nitrophenyl 2-acetamido-6-O-tert-butylphenylsilyl-2-deoxy-β-D-glucopyranoside

There total 1 articles about 4-nitrophenyl 2-acetamido-6-O-tert-butylphenylsilyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 3459-18-5,50645-66-4
4-nitrophenyl N-acetyl-β-D-glucosaminide

: 467448-46-0
4-nitrophenyl 2-acetamido-6-O-tert-butylphenylsilyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With pyridine; at 20 ℃; for 16h;
DOI:10.1016/S0008-6215(02)00104-0

Reference yield: 53.0%

: 108-24-7
acetic anhydride

: 86520-63-0
2,3,4,6-tetra-O-acetyl-α-galactopyranosyl trichloroacetimidate

: 467448-46-0
4-nitrophenyl 2-acetamido-6-O-tert-butylphenylsilyl-2-deoxy-β-D-glucopyranoside

: 467448-47-1
4-nitrophenyl (2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->4)-2-acetamido-3-O-acetyl-6-O-tert-butyl-diphenylsilyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: 2,3,4,6-tetra-O-acetyl-α-galactopyranosyl trichloroacetimidate; 4-nitrophenyl 2-acetamido-6-O-tert-butylphenylsilyl-2-deoxy-β-D-glucopyranoside; In dichloromethane; at 20 ℃; for 2h;

With boron trifluoride diethyl etherate; In dichloromethane; at -30 ℃;

acetic anhydride; With pyridine; at 20 - 48 ℃;
DOI:10.1016/S0008-6215(02)00104-0

Reference yield:

: 467448-46-0
4-nitrophenyl 2-acetamido-6-O-tert-butylphenylsilyl-2-deoxy-β-D-glucopyranoside

: Sulfuric acid mono-[(2S,3R,4R,5R,6R)-3-acetylamino-6-(tert-butyl-diphenyl-silanyloxymethyl)-5-hydroxy-2-(4-nitro-phenoxy)-tetrahydro-pyran-4-yl] ester

: Sulfuric acid mono-[(2R,3S,4R,5R,6S)-5-acetylamino-2-(tert-butyl-diphenyl-silanyloxymethyl)-4-hydroxy-6-(4-nitro-phenoxy)-tetrahydro-pyran-3-yl] ester

Guidance literature:: With Dowex Na-form; sulfur trioxide trimethylamine complex; In N,N-dimethyl-formamide; at 40 ℃; for 10h;
DOI:10.1016/S0960-894X(03)00611-5