(C₅H₅)ReNO{P(C₆H₅)3}(CH₂NC₅H₅)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)ReNOP(C₆H₅)3CH₂NC₅H₅PF₆

Base Information

Chemical Name:(C₅H₅)ReNO{P(C₆H₅)3}(CH₂NC₅H₅)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)ReNOP(C₆H₅)3CH₂NC₅H₅PF₆
CAS No.:71763-30-9
Molecular Formula:C₂₉H₂₇N₂OPRe*F₆P
Molecular Weight:781.691
Hs Code.:

(C<sub>5</sub>H<sub>5</sub>)ReNO{P(C<sub>6</sub>H<sub>5</sub>)3}(CH<sub>2</sub>NC<sub>5</sub>H<sub>5</sub>)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=(C<sub>5</sub>H<sub>5</sub>)ReNOP(C<sub>6</sub>H<sub>5</sub>)3CH<sub>2</sub>NC<sub>5</sub>H<sub>5</sub>PF<sub>6</sub>

Synonyms:(C₅H₅)ReNO{P(C₆H₅)3}(CH₂NC₅H₅)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)ReNOP(C₆H₅)3CH₂NC₅H₅PF₆

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Chemical Property of (C₅H₅)ReNO{P(C₆H₅)3}(CH₂NC₅H₅)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)ReNOP(C₆H₅)3CH₂NC₅H₅PF₆

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Technology Process of (C₅H₅)ReNO{P(C₆H₅)3}(CH₂NC₅H₅)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)ReNOP(C₆H₅)3CH₂NC₅H₅PF₆

There total 3 articles about (C₅H₅)ReNO{P(C₆H₅)3}(CH₂NC₅H₅)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)ReNOP(C₆H₅)3CH₂NC₅H₅PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: (η5-C5H5)(Me)(NO)(PPh3)rhenium(II)

: 437-17-2
tritylium hexafluorophosphate

: 71763-30-9
(C₅H₅)ReNO{P(C₆H₅)3}(CH₂NC₅H₅)⁽¹⁺⁾*PF₆^(1-)=(C₅H₅)ReNOP(C₆H₅)3CH₂NC₅H₅PF₆

Guidance literature:: With pyridine; In dichloromethane; -78°C, 0.5 h, under N2, addn. of pyridine, allowed to warm to room temp.; solvent removed by rotary evapn., residue washed with ethyl ether, recrystn. from CH2Cl2/ethyl ether, elem. anal.;
DOI:10.1021/ja00365a027