[Ph₂CCNInMe₂(tetrahydrofuran)]2

Base Information

Chemical Name:[Ph₂CCNInMe₂(tetrahydrofuran)]2
CAS No.:614760-71-3
Molecular Formula:C₄₀H₄₈In₂N₂O₂
Molecular Weight:818.473
Hs Code.:

[Ph<sub>2</sub>CCNInMe<sub>2</sub>(tetrahydrofuran)]2

Synonyms:[Ph₂CCNInMe₂(tetrahydrofuran)]2

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Chemical Property of [Ph₂CCNInMe₂(tetrahydrofuran)]2

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Technology Process of [Ph₂CCNInMe₂(tetrahydrofuran)]2

There total 2 articles about [Ph₂CCNInMe₂(tetrahydrofuran)]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 86-29-3
Diphenylacetonitrile

: 3385-78-2
trimethyl indium

: 614760-71-3
[Ph₂CCNInMe₂(tetrahydrofuran)]2

Guidance literature:: cesium fluoride; In toluene; byproducts: CH4; under Ar; soln. of InMe3 in toluene dropped into soln. of Ph2CHCN; 1 mol% CsF added; heated under reflux for 48 h; solvent removed under vac.; dissolved in THF; filtered; filtrate stored at -20°C for several d;
DOI:10.1021/om0303956

Reference yield: 87.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 614760-73-5
((C₆H₅)2CCNLi(O(C₂H₅)2)2)2

: 14629-99-3
dimethylindium chloride

: 614760-71-3
[Ph₂CCNInMe₂(tetrahydrofuran)]2

Guidance literature:: In diethyl ether; byproducts: LiCl; under Ar; soln. of Li compd. in Et2O added at 0°C to Me2InCl in Et2O; stirred for 10 h; filtered; filtrate evapd. to dryness; dissolved in THF; stored at -20°C for several d;
DOI:10.1021/om0303956