4-amino-5-{[4-(methanesulfonyl)phenoxy]methyl}-4H-1,2,4-triazole-3-thiol

Base Information

Chemical Name:4-amino-5-{[4-(methanesulfonyl)phenoxy]methyl}-4H-1,2,4-triazole-3-thiol
CAS No.:939980-74-2
Molecular Formula:C₁₀H₁₂N₄O₃S₂
Molecular Weight:300.362
Hs Code.:

Synonyms:4-amino-5-{[4-(methanesulfonyl)phenoxy]methyl}-4H-1,2,4-triazole-3-thiol

Suppliers and Price of 4-amino-5-{[4-(methanesulfonyl)phenoxy]methyl}-4H-1,2,4-triazole-3-thiol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-amino-5-{[4-(methanesulfonyl)phenoxy]methyl}-4H-1,2,4-triazole-3-thiol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-amino-5-{[4-(methanesulfonyl)phenoxy]methyl}-4H-1,2,4-triazole-3-thiol

There total 4 articles about 4-amino-5-{[4-(methanesulfonyl)phenoxy]methyl}-4H-1,2,4-triazole-3-thiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 75-15-0,12122-00-8
carbon disulfide

: 939980-71-9
2-[4-(methylsulphonyl)phenoxy]acetohydrazide

: 939980-74-2
4-amino-5-{[4-(methanesulfonyl)phenoxy]methyl}-4H-1,2,4-triazole-3-thiol

Guidance literature:: carbon disulfide; 2-[4-(methylsulphonyl)phenoxy]acetohydrazide; With potassium hydroxide; In methanol; at 20 ℃;

With hydrazine hydrate; In water; Further stages.; Heating;
DOI:10.1016/j.ejmech.2006.10.010

Reference yield:

: 939980-68-4
ethyl [4-(methanesulfonyl)phenoxy]acetate

: 939980-74-2
4-amino-5-{[4-(methanesulfonyl)phenoxy]methyl}-4H-1,2,4-triazole-3-thiol

Guidance literature:: Multi-step reaction with 2 steps

1.1: 85 percent / hydrazine hydrate / methanol / Heating

2.1: potassium hydroxide / methanol / 20 °C

2.2: 72 percent / hydrazine hydrate / H₂O / Heating

With potassium hydroxide; hydrazine hydrate; In methanol;
DOI:10.1016/j.ejmech.2006.10.010

Reference yield:

: 1073-72-9
4-hydroxythioanisole

: 939980-74-2
4-amino-5-{[4-(methanesulfonyl)phenoxy]methyl}-4H-1,2,4-triazole-3-thiol

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / acetone / 3 h / Heating

2.1: hydrogen peroxide; glacial acetic acid / 3 h / 70 - 75 °C

3.1: 85 percent / hydrazine hydrate / methanol / Heating

4.1: potassium hydroxide / methanol / 20 °C

4.2: 72 percent / hydrazine hydrate / H₂O / Heating

With potassium hydroxide; dihydrogen peroxide; potassium carbonate; hydrazine hydrate; acetic acid; In methanol; acetone;
DOI:10.1016/j.ejmech.2006.10.010