4-methoxy-N,2,6-trimethyl-N-[2-[2-oxo-2-(4-phenyl-4,5,6,7-tetrahydro-1H-imidazo[4,5-c]pyridin-5-yl)-ethoxy]-ethyl]-benzenesulfonic acid amide

Base Information

Chemical Name:4-methoxy-N,2,6-trimethyl-N-[2-[2-oxo-2-(4-phenyl-4,5,6,7-tetrahydro-1H-imidazo[4,5-c]pyridin-5-yl)-ethoxy]-ethyl]-benzenesulfonic acid amide
CAS No.:1190970-46-7
Molecular Formula:C₂₆H₃₂N₄O₅S
Molecular Weight:512.63
Hs Code.:

Synonyms:4-methoxy-N,2,6-trimethyl-N-[2-[2-oxo-2-(4-phenyl-4,5,6,7-tetrahydro-1H-imidazo[4,5-c]pyridin-5-yl)-ethoxy]-ethyl]-benzenesulfonic acid amide

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Chemical Property of 4-methoxy-N,2,6-trimethyl-N-[2-[2-oxo-2-(4-phenyl-4,5,6,7-tetrahydro-1H-imidazo[4,5-c]pyridin-5-yl)-ethoxy]-ethyl]-benzenesulfonic acid amide

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Technology Process of 4-methoxy-N,2,6-trimethyl-N-[2-[2-oxo-2-(4-phenyl-4,5,6,7-tetrahydro-1H-imidazo[4,5-c]pyridin-5-yl)-ethoxy]-ethyl]-benzenesulfonic acid amide

There total 5 articles about 4-methoxy-N,2,6-trimethyl-N-[2-[2-oxo-2-(4-phenyl-4,5,6,7-tetrahydro-1H-imidazo[4,5-c]pyridin-5-yl)-ethoxy]-ethyl]-benzenesulfonic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 766558-33-2
[2-[[(4-methoxy-2,6-dimethylphenyl)sulfonyl]methylamino]ethoxy]acetic acid

: 4875-39-2,62002-37-3,62002-38-4
4-phenylspinaceamine

: 1190970-46-7
4-methoxy-N,2,6-trimethyl-N-[2-[2-oxo-2-(4-phenyl-4,5,6,7-tetrahydro-1H-imidazo[4,5-c]pyridin-5-yl)-ethoxy]-ethyl]-benzenesulfonic acid amide

Guidance literature:: [2-[[(4-methoxy-2,6-dimethylphenyl)sulfonyl]methylamino]ethoxy]acetic acid; With 1,1'-carbonyldiimidazole; In dichloromethane; at 20 ℃; for 1.5h;

4-phenylspinaceamine; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 18h;

Reference yield:

: 766558-31-0
N-(2-hydroxyethyl)-4-methoxy-2,6,N-trimethylbenzenesulphonamide

: 1190970-46-7
4-methoxy-N,2,6-trimethyl-N-[2-[2-oxo-2-(4-phenyl-4,5,6,7-tetrahydro-1H-imidazo[4,5-c]pyridin-5-yl)-ethoxy]-ethyl]-benzenesulfonic acid amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrabutyl-ammonium chloride; sodium hydroxide / water; toluene / 0 - 20 °C

2.1: water; sodium hydroxide / tetrahydrofuran; methanol / 1 h / 20 °C

2.2: 0 °C

3.1: 1,1'-carbonyldiimidazole / dichloromethane / 1.5 h / 20 °C

3.2: 18 h / 20 °C

With tetrabutyl-ammonium chloride; water; 1,1'-carbonyldiimidazole; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; toluene;

Reference yield:

: 766558-32-1
[2-[[(4-methoxy-2,6-dimethylphenyl)sulfonyl]methylamino]ethoxy]acetic acid 1,1-dimethylethyl ester

: 1190970-46-7
4-methoxy-N,2,6-trimethyl-N-[2-[2-oxo-2-(4-phenyl-4,5,6,7-tetrahydro-1H-imidazo[4,5-c]pyridin-5-yl)-ethoxy]-ethyl]-benzenesulfonic acid amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; sodium hydroxide / tetrahydrofuran; methanol / 1 h / 20 °C

1.2: 0 °C

2.1: 1,1'-carbonyldiimidazole / dichloromethane / 1.5 h / 20 °C

2.2: 18 h / 20 °C

With water; 1,1'-carbonyldiimidazole; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane;