2-bromo-4-n-hexyl-3-hydroxy-N-pivaloylaniline

Base Information

Chemical Name:2-bromo-4-n-hexyl-3-hydroxy-N-pivaloylaniline
CAS No.:168335-64-6
Molecular Formula:C₁₇H₂₆BrNO₂
Molecular Weight:356.303
Hs Code.:

Synonyms:2-bromo-4-n-hexyl-3-hydroxy-N-pivaloylaniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-bromo-4-n-hexyl-3-hydroxy-N-pivaloylaniline

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Technology Process of 2-bromo-4-n-hexyl-3-hydroxy-N-pivaloylaniline

There total 4 articles about 2-bromo-4-n-hexyl-3-hydroxy-N-pivaloylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 168335-62-4
N-(2-Bromo-4-hexanoyl-3-hydroxy-phenyl)-2,2-dimethyl-propionamide

: 168335-64-6
2-bromo-4-n-hexyl-3-hydroxy-N-pivaloylaniline

Guidance literature:: With sodium tetrahydroborate; water; chloroformic acid ethyl ester; triethylamine; Yield given. Multistep reaction; 1.) THF, 0 deg C, 30 min, 2.) THF, RT, 3 h;
DOI:10.1021/ja00130a003

Reference yield:

: 56619-93-3
N-(3-methoxyphenyl)pivalamide

: 168335-64-6
2-bromo-4-n-hexyl-3-hydroxy-N-pivaloylaniline

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi, 2.) bromine / 1.) THF, hexane, 0 deg C, 2.5 h, 2.) THF, hexane, -78 deg C, 1 h

2: 1.) AlCl₃ / 1.) CS₂, reflux, 3 h, 2.) 70 deg C, 2 d

3: 1.) triethylamine, ethyl chloroformate, 2.) sodium borohydride, water / 1.) THF, 0 deg C, 30 min, 2.) THF, RT, 3 h

With sodium tetrahydroborate; n-butyllithium; aluminium trichloride; water; bromine; chloroformic acid ethyl ester; triethylamine;
DOI:10.1021/ja00130a003

Reference yield:

: 168335-61-3
N-(2-bromo-3-methoxyphenyl)-2,2-dimethylpropionamide

: 168335-64-6
2-bromo-4-n-hexyl-3-hydroxy-N-pivaloylaniline

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) AlCl₃ / 1.) CS₂, reflux, 3 h, 2.) 70 deg C, 2 d

2: 1.) triethylamine, ethyl chloroformate, 2.) sodium borohydride, water / 1.) THF, 0 deg C, 30 min, 2.) THF, RT, 3 h

With sodium tetrahydroborate; aluminium trichloride; water; chloroformic acid ethyl ester; triethylamine;
DOI:10.1021/ja00130a003