5-<3-(4-benzyloxybenzyloxy)benzyl>-1-<(2-benzoyloxyethoxy)methyl>-2-keto-4-methoxypyrimidine

Base Information

Chemical Name:5-<3-(4-benzyloxybenzyloxy)benzyl>-1-<(2-benzoyloxyethoxy)methyl>-2-keto-4-methoxypyrimidine
CAS No.:110522-20-8
Molecular Formula:C₃₆H₃₄N₂O₇
Molecular Weight:606.675
Hs Code.:

Synonyms:5-<3-(4-benzyloxybenzyloxy)benzyl>-1-<(2-benzoyloxyethoxy)methyl>-2-keto-4-methoxypyrimidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-<3-(4-benzyloxybenzyloxy)benzyl>-1-<(2-benzoyloxyethoxy)methyl>-2-keto-4-methoxypyrimidine

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Technology Process of 5-<3-(4-benzyloxybenzyloxy)benzyl>-1-<(2-benzoyloxyethoxy)methyl>-2-keto-4-methoxypyrimidine

There total 2 articles about 5-<3-(4-benzyloxybenzyloxy)benzyl>-1-<(2-benzoyloxyethoxy)methyl>-2-keto-4-methoxypyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 110522-19-5
5-(3-hydroxybenzyl)-1-<(2-benzoyloxyethoxy)methyl>-2-keto-4-methoxypyrimidine

: 836-42-0
4-benzyloxybenzyl chloride

: 110522-20-8
5-<3-(4-benzyloxybenzyloxy)benzyl>-1-<(2-benzoyloxyethoxy)methyl>-2-keto-4-methoxypyrimidine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 40 ℃; overnight;
DOI:10.1002/jhet.5570230609

Reference yield:

: 110522-18-4
Benzoic acid 2-[5-(3-benzyloxy-benzyl)-4-methoxy-2-oxo-2H-pyrimidin-1-ylmethoxy]-ethyl ester

: 110522-20-8
5-<3-(4-benzyloxybenzyloxy)benzyl>-1-<(2-benzoyloxyethoxy)methyl>-2-keto-4-methoxypyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / 6N aq. HCl, H₂ / Pd/C / methanol / 1 h / 2206.5 Torr

2: 70 percent / potassium carbonate / dimethylformamide / 40 °C / overnight

With hydrogenchloride; hydrogen; potassium carbonate; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570230609