3’-4’-dichloro-N-((4-(4-ethoxyphenoxy)phenyl)sulfonyl)[1,1’-biphenyl]-3-carboxamide

Base Information

Chemical Name:3’-4’-dichloro-N-((4-(4-ethoxyphenoxy)phenyl)sulfonyl)[1,1’-biphenyl]-3-carboxamide
CAS No.:1326777-62-1
Molecular Formula:C₂₇H₂₁Cl₂NO₅S
Molecular Weight:542.439
Hs Code.:

Synonyms:3’-4’-dichloro-N-((4-(4-ethoxyphenoxy)phenyl)sulfonyl)[1,1’-biphenyl]-3-carboxamide

Suppliers and Price of 3’-4’-dichloro-N-((4-(4-ethoxyphenoxy)phenyl)sulfonyl)[1,1’-biphenyl]-3-carboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3’-4’-dichloro-N-((4-(4-ethoxyphenoxy)phenyl)sulfonyl)[1,1’-biphenyl]-3-carboxamide

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Technology Process of 3’-4’-dichloro-N-((4-(4-ethoxyphenoxy)phenyl)sulfonyl)[1,1’-biphenyl]-3-carboxamide

There total 6 articles about 3’-4’-dichloro-N-((4-(4-ethoxyphenoxy)phenyl)sulfonyl)[1,1’-biphenyl]-3-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1097096-19-9
4-(4-ethoxyphenoxy)benzenesulfonamide

: 3-(3,4-dichlorophenyl)benzoyl chloride

: 1326777-62-1
3’-4’-dichloro-N-((4-(4-ethoxyphenoxy)phenyl)sulfonyl)[1,1’-biphenyl]-3-carboxamide

Guidance literature:: With dmap; triethylamine; In ethyl acetate; toluene; at 55 ℃; for 5h; Inert atmosphere;
DOI:10.1021/acs.orglett.8b02819

Reference yield:

: 844878-91-7
3',4'-dichloro[1,1‘-biphenyl]-3-carboxylic acid

: 1326777-62-1
3’-4’-dichloro-N-((4-(4-ethoxyphenoxy)phenyl)sulfonyl)[1,1’-biphenyl]-3-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide; oxalyl dichloride / tetrahydrofuran / Inert atmosphere

2: triethylamine; dmap / ethyl acetate; toluene / 5 h / 55 °C / Inert atmosphere

With dmap; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; ethyl acetate; toluene;
DOI:10.1021/acs.orglett.8b02819

Reference yield:

: 618-51-9
3-Iodobenzoic acid

: 1326777-62-1
3’-4’-dichloro-N-((4-(4-ethoxyphenoxy)phenyl)sulfonyl)[1,1’-biphenyl]-3-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: palladium diacetate; triphenylphosphine; sodium carbonate / 1,2-dimethoxyethane; water / 21 h / 56 - 80 °C / Inert atmosphere

2: N,N-dimethyl-formamide; oxalyl dichloride / tetrahydrofuran / Inert atmosphere

3: triethylamine; dmap / ethyl acetate; toluene / 5 h / 55 °C / Inert atmosphere

With dmap; oxalyl dichloride; palladium diacetate; sodium carbonate; triethylamine; N,N-dimethyl-formamide; triphenylphosphine; In tetrahydrofuran; 1,2-dimethoxyethane; water; ethyl acetate; toluene;
DOI:10.1021/acs.orglett.8b02819