N-(allyloxycarbonyl)-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-galactopyranosyl)-L-serilvalylphenylalanine (methoxyethoxy)ethyl ester

Base Information

Chemical Name:N-(allyloxycarbonyl)-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-galactopyranosyl)-L-serilvalylphenylalanine (methoxyethoxy)ethyl ester
CAS No.:156311-02-3
Molecular Formula:C₄₀H₅₈N₄O₁₇
Molecular Weight:866.917
Hs Code.:

Synonyms:N-(allyloxycarbonyl)-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-galactopyranosyl)-L-serilvalylphenylalanine (methoxyethoxy)ethyl ester

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Chemical Property of N-(allyloxycarbonyl)-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-galactopyranosyl)-L-serilvalylphenylalanine (methoxyethoxy)ethyl ester

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Technology Process of N-(allyloxycarbonyl)-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-galactopyranosyl)-L-serilvalylphenylalanine (methoxyethoxy)ethyl ester

There total 12 articles about N-(allyloxycarbonyl)-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-galactopyranosyl)-L-serilvalylphenylalanine (methoxyethoxy)ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 126133-70-8
N-(allyloxycarbonyl)-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-galactopyranosyl)-L-serine

: 197727-46-1
(S)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-phenyl-propionic acid 2-(2-methoxy-ethoxy)-ethyl ester

: 156311-02-3
N-(allyloxycarbonyl)-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-galactopyranosyl)-L-serilvalylphenylalanine (methoxyethoxy)ethyl ester

Guidance literature:: With O-<[cyano(ethoxycarbonyl)methylene]amino>-1,1,3,3-tetramethyluronium tetrafluoroborate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 1h; Ambient temperature;
DOI:10.1021/jo951899j

Reference yield: 67.0%

: 126133-70-8
N-(allyloxycarbonyl)-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-galactopyranosyl)-L-serine

: (S)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-phenyl-propionic acid 2-(2-methoxy-ethoxy)-ethyl ester; hydrochloride

: 156311-02-3
N-(allyloxycarbonyl)-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-galactopyranosyl)-L-serilvalylphenylalanine (methoxyethoxy)ethyl ester

Guidance literature:: With O-<[cyano(ethoxycarbonyl)methylene]amino>-1,1,3,3-tetramethyluronium tetrafluoroborate; benzotriazol-1-ol;

Reference yield:

: 13734-41-3
t-Boc-L-valine

: 156311-02-3
N-(allyloxycarbonyl)-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-galactopyranosyl)-L-serilvalylphenylalanine (methoxyethoxy)ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / i-Pr₂NEt, EEDQ / CH₂Cl₂ / 12 h / Ambient temperature

2: 87 percent / HCl/Et₂O / 4 h / Ambient temperature

3: 67 percent / O-<(cyano(ethoxycarbonyl)methylidene)amino>-1,1,3,3-tetramethyluronium tetrafluoroborate, HOBt, i-Pr₂NEt / dimethylformamide / 1 h / Ambient temperature

With hydrogenchloride; O-<[cyano(ethoxycarbonyl)methylene]amino>-1,1,3,3-tetramethyluronium tetrafluoroborate; diethyl ether; benzotriazol-1-ol; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo951899j