N-(1-cyclohexyl-3-oxo-2-phenyl-2,3-dihydro-1H-indazole-5-carbonyl)-4-methoxybenzenesulfonamide

Base Information

Chemical Name:N-(1-cyclohexyl-3-oxo-2-phenyl-2,3-dihydro-1H-indazole-5-carbonyl)-4-methoxybenzenesulfonamide
CAS No.:1086027-32-8
Molecular Formula:C₂₇H₂₇N₃O₅S
Molecular Weight:505.594
Hs Code.:

Synonyms:N-(1-cyclohexyl-3-oxo-2-phenyl-2,3-dihydro-1H-indazole-5-carbonyl)-4-methoxybenzenesulfonamide

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Chemical Property of N-(1-cyclohexyl-3-oxo-2-phenyl-2,3-dihydro-1H-indazole-5-carbonyl)-4-methoxybenzenesulfonamide

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Technology Process of N-(1-cyclohexyl-3-oxo-2-phenyl-2,3-dihydro-1H-indazole-5-carbonyl)-4-methoxybenzenesulfonamide

There total 10 articles about N-(1-cyclohexyl-3-oxo-2-phenyl-2,3-dihydro-1H-indazole-5-carbonyl)-4-methoxybenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1086024-43-2
1-cyclohexyl-3-oxo-2-phenyl-2,3-dihydro-1H-indazole-5-carboxylic acid

: 1129-26-6
4-methoxybenzene sulfonamide

: 1086027-32-8
N-(1-cyclohexyl-3-oxo-2-phenyl-2,3-dihydro-1H-indazole-5-carbonyl)-4-methoxybenzenesulfonamide

Guidance literature:: With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane;

Reference yield:

: 1086031-04-0
C₂₁H₂₆N₂O₄

: 1086027-32-8
N-(1-cyclohexyl-3-oxo-2-phenyl-2,3-dihydro-1H-indazole-5-carbonyl)-4-methoxybenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: pyridinium p-toluenesulfonate / toluene / 0.5 h / 90 °C

2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1,4-dioxane / 3 h / 110 °C / Heating / reflux

3: sodium hydroxide; water / methanol / 1 h / 60 °C

4: dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide / dichloromethane

With dmap; sodium hydroxide; water; pyridinium p-toluenesulfonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,4-dioxane; methanol; dichloromethane; toluene;

Reference yield:

: 1086030-13-8
1-cyclohexyl-5-methyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazole-4-carbaldehyde

: 1086027-32-8
N-(1-cyclohexyl-3-oxo-2-phenyl-2,3-dihydro-1H-indazole-5-carbonyl)-4-methoxybenzenesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium; diisopropylamine / tetrahydrofuran; n-heptane / 2.33 h / -78 - 0 °C

1.2: -78 - 50 °C

2.1: pyridinium p-toluenesulfonate / toluene / 0.5 h / 90 °C

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1,4-dioxane / 3 h / 110 °C / Heating / reflux

4.1: sodium hydroxide; water / methanol / 1 h / 60 °C

5.1: dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide / dichloromethane

With dmap; sodium hydroxide; n-butyllithium; water; pyridinium p-toluenesulfonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; 1,4-dioxane; methanol; n-heptane; dichloromethane; toluene;