propane-1,3-diyl bis[3-(3-methoxyphenyl)-1,6,6-trimethyl-5-oxo-2,7-dioxabicyclo[2.2.1]heptane-4-carboxylate]

Base Information

Chemical Name:propane-1,3-diyl bis[3-(3-methoxyphenyl)-1,6,6-trimethyl-5-oxo-2,7-dioxabicyclo[2.2.1]heptane-4-carboxylate]
CAS No.:1453500-67-8
Molecular Formula:C₃₅H₄₀O₁₂
Molecular Weight:652.695
Hs Code.:

Synonyms:propane-1,3-diyl bis[3-(3-methoxyphenyl)-1,6,6-trimethyl-5-oxo-2,7-dioxabicyclo[2.2.1]heptane-4-carboxylate]

Suppliers and Price of propane-1,3-diyl bis[3-(3-methoxyphenyl)-1,6,6-trimethyl-5-oxo-2,7-dioxabicyclo[2.2.1]heptane-4-carboxylate]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of propane-1,3-diyl bis[3-(3-methoxyphenyl)-1,6,6-trimethyl-5-oxo-2,7-dioxabicyclo[2.2.1]heptane-4-carboxylate]

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Technology Process of propane-1,3-diyl bis[3-(3-methoxyphenyl)-1,6,6-trimethyl-5-oxo-2,7-dioxabicyclo[2.2.1]heptane-4-carboxylate]

There total 2 articles about propane-1,3-diyl bis[3-(3-methoxyphenyl)-1,6,6-trimethyl-5-oxo-2,7-dioxabicyclo[2.2.1]heptane-4-carboxylate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1453500-83-8
propane-1,3-diyl bis(2-diazo-4,4-dimethyl-3,5-dioxohexanoate)

: 591-31-1
3-methoxy-benzaldehyde

: 1453500-67-8
propane-1,3-diyl bis[3-(3-methoxyphenyl)-1,6,6-trimethyl-5-oxo-2,7-dioxabicyclo[2.2.1]heptane-4-carboxylate]

Guidance literature:: With dirhodium tetraacetate; In benzene; for 1h; Inert atmosphere; Reflux;
DOI:10.1055/s-0033-1338801

Reference yield:

: 1453500-79-2
propane-1,3-diyl bis(4,4-dimethyl-3,5-dioxohexanoate)

: 1453500-67-8
propane-1,3-diyl bis[3-(3-methoxyphenyl)-1,6,6-trimethyl-5-oxo-2,7-dioxabicyclo[2.2.1]heptane-4-carboxylate]

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; Methanesulfonyl azide / dichloromethane / 0 °C / Inert atmosphere

2: dirhodium tetraacetate / benzene / 1 h / Inert atmosphere; Reflux

With dirhodium tetraacetate; triethylamine; Methanesulfonyl azide; In dichloromethane; benzene;
DOI:10.1055/s-0033-1338801