(S)-2-(4-nitrophenyl)-1-[(thiophen-2-yl)oxazol-4-yl]ethanamine hydrobromide salt

Base Information

Chemical Name:(S)-2-(4-nitrophenyl)-1-[(thiophen-2-yl)oxazol-4-yl]ethanamine hydrobromide salt
CAS No.:1000395-37-8
Molecular Formula:BrH*C₁₅H₁₃N₃O₃S
Molecular Weight:396.264
Hs Code.:

Synonyms:(S)-2-(4-nitrophenyl)-1-[(thiophen-2-yl)oxazol-4-yl]ethanamine hydrobromide salt

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Chemical Property of (S)-2-(4-nitrophenyl)-1-[(thiophen-2-yl)oxazol-4-yl]ethanamine hydrobromide salt

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Technology Process of (S)-2-(4-nitrophenyl)-1-[(thiophen-2-yl)oxazol-4-yl]ethanamine hydrobromide salt

There total 3 articles about (S)-2-(4-nitrophenyl)-1-[(thiophen-2-yl)oxazol-4-yl]ethanamine hydrobromide salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5813-89-8
2-thiophenylcarboxamide

: 293291-20-0
(S)-tert-butyl 4-bromo-1-(4-nitrophenyl)-3-oxobutan-2-ylcarbamate

: 1000395-37-8
(S)-2-(4-nitrophenyl)-1-[(thiophen-2-yl)oxazol-4-yl]ethanamine hydrobromide salt

Guidance literature:: In acetonitrile; for 5h; Reflux;

Reference yield:

: 33305-77-0
Boc-Phe(p-NO₂)-OH

: 1000395-37-8
(S)-2-(4-nitrophenyl)-1-[(thiophen-2-yl)oxazol-4-yl]ethanamine hydrobromide salt

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; isobutyl chloroformate / tetrahydrofuran / 0.33 h / 0 °C

1.2: 3 h / 0 - 20 °C

2.1: hydrogen bromide / water; tetrahydrofuran / 1.5 h / 0 °C

3.1: acetonitrile / 5 h / Reflux

With hydrogen bromide; triethylamine; isobutyl chloroformate; In tetrahydrofuran; water; acetonitrile;

Reference yield:

: 127106-74-5
(S)-[3-diazo-1-(4-nitrobenzyl)-2-oxo-propyl]carbamic acid tert-butyl ester

: 1000395-37-8
(S)-2-(4-nitrophenyl)-1-[(thiophen-2-yl)oxazol-4-yl]ethanamine hydrobromide salt

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen bromide / water; tetrahydrofuran / 1.5 h / 0 °C

2: acetonitrile / 5 h / Reflux

With hydrogen bromide; In tetrahydrofuran; water; acetonitrile;