N-methyl dimethyl-1,4 diepoxy-1,8a:4,4a ethano-5,8 octahydro-1,2,3,4,4a,5,8,8a naphtalene dicarboximide-9,10 syn

Base Information

• Chemical Name: N-methyl dimethyl-1,4 diepoxy-1,8a:4,4a ethano-5,8 octahydro-1,2,3,4,4a,5,8,8a naphtalene dicarboximide-9,10 syn
• CAS No.: 94082-90-3
• Molecular Formula: C₁₇H₁₉NO₄
• Molecular Weight: 301.342

Synonyms:N-methyl dimethyl-1,4 diepoxy-1,8a:4,4a ethano-5,8 octahydro-1,2,3,4,4a,5,8,8a naphtalene dicarboximide-9,10 syn

Chemical Property of N-methyl dimethyl-1,4 diepoxy-1,8a:4,4a ethano-5,8 octahydro-1,2,3,4,4a,5,8,8a naphtalene dicarboximide-9,10 syn

Chemical Property:

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Technology Process of N-methyl dimethyl-1,4 diepoxy-1,8a:4,4a ethano-5,8 octahydro-1,2,3,4,4a,5,8,8a naphtalene dicarboximide-9,10 syn

There total 2 articles about N-methyl dimethyl-1,4 diepoxy-1,8a:4,4a ethano-5,8 octahydro-1,2,3,4,4a,5,8,8a naphtalene dicarboximide-9,10 syn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

N-methylmaleimide (930-88-1) + 1,4-epidioxy-1,4-dimethyl-1,2,3,4-tetrahydronaphthalene (63797-42-2) → 1,2-diacetylbenzene (704-00-7) + 2,5-epoxy-2,5-dimethyl-2,3,4,5-tetrahydro-benzooxepine (94082-89-0) + N-methyl dimethyl-1,4 diepoxy-1,8a:4,4a ethano-5,8 octahydro-1,2,3,4,4a,5,8,8a naphtalene dicarboximide-9,10 syn (94082-90-3)

Guidance literature:

In benzene; for 9h; Product distribution; Ambient temperature; Irradiation; without irradiation, other temperatures, other times;

Reference yield: 10.0%

1,4-epidioxy-1,4-dimethyl-1,2,3,4-tetrahydronaphthalene (63797-42-2) → 1,2-diacetylbenzene (704-00-7) + 1,4-dimethylnaphthalene (571-58-4) + 2,5-epoxy-2,5-dimethyl-2,3,4,5-tetrahydro-benzooxepine (94082-89-0) + N-methyl dimethyl-1,4 diepoxy-1,8a:4,4a ethano-5,8 octahydro-1,2,3,4,4a,5,8,8a naphtalene dicarboximide-9,10 syn (94082-90-3)

Guidance literature:

With N-methylmaleimide; In various solvent(s); for 5h; Heating;

upstream raw materials:

N-methylmaleimide

1,4-epidioxy-1,4-dimethyl-1,2,3,4-tetrahydronaphthalene

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