methyl 2-<2-hydroxy-3-<<2-<<(phenylamino)carbonyl>amino>ethyl>amino>propoxy>benzoate

Base Information

Chemical Name:methyl 2-<2-hydroxy-3-<<2-<<(phenylamino)carbonyl>amino>ethyl>amino>propoxy>benzoate
CAS No.:83019-57-2
Molecular Formula:C₂₀H₂₅N₃O₅
Molecular Weight:387.436
Hs Code.:

Synonyms:methyl 2-<2-hydroxy-3-<<2-<<(phenylamino)carbonyl>amino>ethyl>amino>propoxy>benzoate

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Chemical Property of methyl 2-<2-hydroxy-3-<<2-<<(phenylamino)carbonyl>amino>ethyl>amino>propoxy>benzoate

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Technology Process of methyl 2-<2-hydroxy-3-<<2-<<(phenylamino)carbonyl>amino>ethyl>amino>propoxy>benzoate

There total 7 articles about methyl 2-<2-hydroxy-3-<<2-<<(phenylamino)carbonyl>amino>ethyl>amino>propoxy>benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

: 85850-48-2
2-<<(phenylamino)carbonyl>amino>ethylamine hydrochloride

: 22589-46-4
1,2-epoxy-3-<2-(methoxycarbonyl)phenoxy>propane

: 83019-57-2
methyl 2-<2-hydroxy-3-<<2-<<(phenylamino)carbonyl>amino>ethyl>amino>propoxy>benzoate

Guidance literature:: With triethylamine; In methanol; for 4h; Heating;
DOI:10.1021/jm00362a004

Reference yield:

: 2-(3-{Benzyl-[2-(3-phenyl-ureido)-ethyl]-amino}-2-hydroxy-propoxy)-benzoic acid methyl ester

: 83019-57-2
methyl 2-<2-hydroxy-3-<<2-<<(phenylamino)carbonyl>amino>ethyl>amino>propoxy>benzoate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 5h; under 760 Torr; Yield given;
DOI:10.1021/jm00353a004

Reference yield:

: 56443-68-6
1-<2-(benzylamino)ethyl>-3-phenylurea

: 83019-57-2
methyl 2-<2-hydroxy-3-<<2-<<(phenylamino)carbonyl>amino>ethyl>amino>propoxy>benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: propan-2-ol / 18 h / Heating

2: H₂ / 30percent Pd/C / ethanol / 5 h / 760 Torr

With hydrogen; palladium on activated charcoal; In ethanol; isopropyl alcohol;
DOI:10.1021/jm00353a004