Technology Process of C25H30O5
There total 6 articles about C25H30O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine; dmap;
In
dichloromethane;
at 20 ℃;
for 12h;
Inert atmosphere;
DOI:10.3987/COM-10-S(E)93
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: lithium aluminium tetrahydride / diethyl ether / 0 - 20 °C / Inert atmosphere
2.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 0 - 20 °C / Inert atmosphere
2.2: 0 - 20 °C / Inert atmosphere
3.1: potassium osmate(VI) dihydrate; 4-methylmorpholine N-oxide / water; acetone / 12 h / 20 °C / Inert atmosphere
4.1: sodium periodate / tetrahydrofuran; water / 0 - 20 °C / Inert atmosphere
5.1: tert.-butyl lithium / tetrahydrofuran; pentane / -78 - 0 °C / Inert atmosphere
5.2: 1 h / -78 °C / Inert atmosphere
6.1: pyridine; dmap / dichloromethane / 12 h / 20 °C / Inert atmosphere
With
pyridine; dmap; potassium osmate(VI) dihydrate; sodium periodate; lithium aluminium tetrahydride; tert.-butyl lithium; sodium hydride; 4-methylmorpholine N-oxide;
In
tetrahydrofuran; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; acetone; mineral oil; pentane;
DOI:10.3987/COM-10-S(E)93
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium osmate(VI) dihydrate; 4-methylmorpholine N-oxide / water; acetone / 12 h / 20 °C / Inert atmosphere
2.1: sodium periodate / tetrahydrofuran; water / 0 - 20 °C / Inert atmosphere
3.1: tert.-butyl lithium / tetrahydrofuran; pentane / -78 - 0 °C / Inert atmosphere
3.2: 1 h / -78 °C / Inert atmosphere
4.1: pyridine; dmap / dichloromethane / 12 h / 20 °C / Inert atmosphere
With
pyridine; dmap; potassium osmate(VI) dihydrate; sodium periodate; tert.-butyl lithium; 4-methylmorpholine N-oxide;
In
tetrahydrofuran; dichloromethane; water; acetone; pentane;
DOI:10.3987/COM-10-S(E)93