(2R)-2-benzyloxyamino-2-phenylcyclohexanone (1'R,2'R)-1',2'-dimethylethylene acetal

Base Information

Chemical Name:(2R)-2-benzyloxyamino-2-phenylcyclohexanone (1'R,2'R)-1',2'-dimethylethylene acetal
CAS No.:1174527-47-9
Molecular Formula:C₂₃H₂₉NO₃
Molecular Weight:367.488
Hs Code.:

Synonyms:(2R)-2-benzyloxyamino-2-phenylcyclohexanone (1'R,2'R)-1',2'-dimethylethylene acetal

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Chemical Property of (2R)-2-benzyloxyamino-2-phenylcyclohexanone (1'R,2'R)-1',2'-dimethylethylene acetal

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Technology Process of (2R)-2-benzyloxyamino-2-phenylcyclohexanone (1'R,2'R)-1',2'-dimethylethylene acetal

There total 1 articles about (2R)-2-benzyloxyamino-2-phenylcyclohexanone (1'R,2'R)-1',2'-dimethylethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1174527-45-7
2-benzyloxyiminocyclohexanone (1R,2R)-1,2-dimethylethylene acetal

: 591-51-5
phenyllithium

: (2S)-2-benzyloxyamino-2-phenylcyclohexanone (1'R,2'R)-1',2'-dimethylethylene acetal

: 1174527-47-9
(2R)-2-benzyloxyamino-2-phenylcyclohexanone (1'R,2'R)-1',2'-dimethylethylene acetal

Guidance literature:: 2-benzyloxyiminocyclohexanone (1R,2R)-1,2-dimethylethylene acetal; phenyllithium; In toluene; at -78 - -17 ℃; Inert atmosphere;

With water; sodium hydrogencarbonate; In toluene; at -7 ℃; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2009.05.004

Reference yield: 92.0%

: 1174527-47-9
(2R)-2-benzyloxyamino-2-phenylcyclohexanone (1'R,2'R)-1',2'-dimethylethylene acetal

: 1174527-48-0
(2R)-2-benzyloxyamino-2-phenylcyclohexanone

Guidance literature:: (2R)-2-benzyloxyamino-2-phenylcyclohexanone (1'R,2'R)-1',2'-dimethylethylene acetal; With hydrogenchloride; water; In methanol; at 50 ℃; Inert atmosphere;

With potassium carbonate; In water; Inert atmosphere;
DOI:10.1016/j.tet.2009.05.004