8-benzenesulfonylmethyl-6-[(tert-butyl-dimethyl-silanyl)-amino]-7-(tert-butyl-dimethyl-silanyloxy)-4H-benzo[1,4]thiazin-3-one

Base Information

Chemical Name:8-benzenesulfonylmethyl-6-[(tert-butyl-dimethyl-silanyl)-amino]-7-(tert-butyl-dimethyl-silanyloxy)-4H-benzo[1,4]thiazin-3-one
CAS No.:251089-55-1
Molecular Formula:C₂₇H₄₂N₂O₄S₂Si₂
Molecular Weight:578.944
Hs Code.:

8-benzenesulfonylmethyl-6-[(<i>tert</i>-butyl-dimethyl-silanyl)-amino]-7-(<i>tert</i>-butyl-dimethyl-silanyloxy)-4<i>H</i>-benzo[1,4]thiazin-3-one

Synonyms:8-benzenesulfonylmethyl-6-[(tert-butyl-dimethyl-silanyl)-amino]-7-(tert-butyl-dimethyl-silanyloxy)-4H-benzo[1,4]thiazin-3-one

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Chemical Property of 8-benzenesulfonylmethyl-6-[(tert-butyl-dimethyl-silanyl)-amino]-7-(tert-butyl-dimethyl-silanyloxy)-4H-benzo[1,4]thiazin-3-one

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Technology Process of 8-benzenesulfonylmethyl-6-[(tert-butyl-dimethyl-silanyl)-amino]-7-(tert-butyl-dimethyl-silanyloxy)-4H-benzo[1,4]thiazin-3-one

There total 8 articles about 8-benzenesulfonylmethyl-6-[(tert-butyl-dimethyl-silanyl)-amino]-7-(tert-butyl-dimethyl-silanyloxy)-4H-benzo[1,4]thiazin-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 69739-34-0
t-butyldimethylsiyl triflate

: 251089-76-6
6-amino-8-benzenesulfonylmethyl-7-hydroxy-4H-benzo[1,4]thiazin-3-one

: 251089-55-1
8-benzenesulfonylmethyl-6-[(tert-butyl-dimethyl-silanyl)-amino]-7-(tert-butyl-dimethyl-silanyloxy)-4H-benzo[1,4]thiazin-3-one

Guidance literature:: In N,N-dimethyl-formamide;
DOI:10.1021/ol991049g

Reference yield:

: 178747-79-0
methyl 2-fluoro-6-methoxybenzoate

: 251089-55-1
8-benzenesulfonylmethyl-6-[(tert-butyl-dimethyl-silanyl)-amino]-7-(tert-butyl-dimethyl-silanyloxy)-4H-benzo[1,4]thiazin-3-one

Guidance literature:: Multi-step reaction with 9 steps

1: 95 percent / NO₂BF₄

2: SnCl₂; aq. HCl

3: 60 percent / LiBEt₃H; 15-crown-5 / tetrahydrofuran

4: DMAP

5: NaI

6: 85 percent / BBr₃ / CH₂Cl₂

7: 100 percent / dimethylformamide

With hydrogenchloride; dmap; nitronium tetrafluoborate; 15-crown-5; boron tribromide; lithium triethylborohydride; sodium iodide; tin(ll) chloride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol991049g

Reference yield:

: 251089-58-4
2-fluoro-6-methoxy-3,5-dinitro-benzoic acid methyl ester

: 251089-55-1
8-benzenesulfonylmethyl-6-[(tert-butyl-dimethyl-silanyl)-amino]-7-(tert-butyl-dimethyl-silanyloxy)-4H-benzo[1,4]thiazin-3-one

Guidance literature:: Multi-step reaction with 8 steps

1: SnCl₂; aq. HCl

2: 60 percent / LiBEt₃H; 15-crown-5 / tetrahydrofuran

3: DMAP

4: NaI

5: 85 percent / BBr₃ / CH₂Cl₂

6: 100 percent / dimethylformamide

With hydrogenchloride; dmap; 15-crown-5; boron tribromide; lithium triethylborohydride; sodium iodide; tin(ll) chloride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol991049g