(+/-)-tert-butyl 3-(triisopropylsilyloxy)-4-(2-(4-(triisopropylsilyloxy)phenethyl)-1,3-dithian-2-yl)butanoate

Base Information

Chemical Name:(+/-)-tert-butyl 3-(triisopropylsilyloxy)-4-(2-(4-(triisopropylsilyloxy)phenethyl)-1,3-dithian-2-yl)butanoate
CAS No.:1240715-20-1
Molecular Formula:C₃₈H₇₀O₄S₂Si₂
Molecular Weight:711.274
Hs Code.:

Synonyms:(+/-)-tert-butyl 3-(triisopropylsilyloxy)-4-(2-(4-(triisopropylsilyloxy)phenethyl)-1,3-dithian-2-yl)butanoate

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Chemical Property of (+/-)-tert-butyl 3-(triisopropylsilyloxy)-4-(2-(4-(triisopropylsilyloxy)phenethyl)-1,3-dithian-2-yl)butanoate

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Technology Process of (+/-)-tert-butyl 3-(triisopropylsilyloxy)-4-(2-(4-(triisopropylsilyloxy)phenethyl)-1,3-dithian-2-yl)butanoate

There total 1 articles about (+/-)-tert-butyl 3-(triisopropylsilyloxy)-4-(2-(4-(triisopropylsilyloxy)phenethyl)-1,3-dithian-2-yl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: (+/-)-tert-butyl 3-hydroxy-4-(2-(4-hydroxyphenethyl)-1,3-dithian-2-yl)butanoate

: 13154-24-0
triisopropylsilyl chloride

: 1240715-20-1
(+/-)-tert-butyl 3-(triisopropylsilyloxy)-4-(2-(4-(triisopropylsilyloxy)phenethyl)-1,3-dithian-2-yl)butanoate

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 0 ℃; for 18h; Inert atmosphere;
DOI:10.1016/j.tet.2010.04.135

Reference yield: 82.0%

: 1240715-20-1
(+/-)-tert-butyl 3-(triisopropylsilyloxy)-4-(2-(4-(triisopropylsilyloxy)phenethyl)-1,3-dithian-2-yl)butanoate

: 1240715-23-4
(+/-)-3-(triisopropylsilyloxy)-4-(2-(4-(triisopropylsilyloxy)phenethyl)-1,3-dithian-2-yl)butanal

Guidance literature:: (+/-)-tert-butyl 3-(triisopropylsilyloxy)-4-(2-(4-(triisopropylsilyloxy)phenethyl)-1,3-dithian-2-yl)butanoate; With diisobutylaluminium hydride; In toluene; at -78 ℃; Inert atmosphere;

With water; sodium hydroxide; In methanol; toluene; at 20 ℃;
DOI:10.1016/j.tet.2010.04.135