tert-butyl (2E)-3-[2-[3-(acetoxymethyl)pyrrolidin-1-yl)-5-[4-(2-butoxyethoxy)phenyl]pyridin-3-yl]-2-methylacrylate

Base Information

Chemical Name:tert-butyl (2E)-3-[2-[3-(acetoxymethyl)pyrrolidin-1-yl)-5-[4-(2-butoxyethoxy)phenyl]pyridin-3-yl]-2-methylacrylate
CAS No.:742100-85-2
Molecular Formula:C₃₂H₄₄N₂O₆
Molecular Weight:552.711
Hs Code.:

Synonyms:tert-butyl (2E)-3-[2-[3-(acetoxymethyl)pyrrolidin-1-yl)-5-[4-(2-butoxyethoxy)phenyl]pyridin-3-yl]-2-methylacrylate

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Chemical Property of tert-butyl (2E)-3-[2-[3-(acetoxymethyl)pyrrolidin-1-yl)-5-[4-(2-butoxyethoxy)phenyl]pyridin-3-yl]-2-methylacrylate

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Technology Process of tert-butyl (2E)-3-[2-[3-(acetoxymethyl)pyrrolidin-1-yl)-5-[4-(2-butoxyethoxy)phenyl]pyridin-3-yl]-2-methylacrylate

There total 1 articles about tert-butyl (2E)-3-[2-[3-(acetoxymethyl)pyrrolidin-1-yl)-5-[4-(2-butoxyethoxy)phenyl]pyridin-3-yl]-2-methylacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 742100-84-1
tert-butyl (2E)-3-[2-[3-(acetoxymethyl)pyrrolidin-1-yl]-5-bromopyridin-3-yl]-2-methylacrylate

: 313747-57-8
4-(2-butoxyethoxy)phenylboric acid

: 742100-85-2
tert-butyl (2E)-3-[2-[3-(acetoxymethyl)pyrrolidin-1-yl)-5-[4-(2-butoxyethoxy)phenyl]pyridin-3-yl]-2-methylacrylate

Guidance literature:: tert-butyl (2E)-3-[2-[3-(acetoxymethyl)pyrrolidin-1-yl]-5-bromopyridin-3-yl]-2-methylacrylate; 4-(2-butoxyethoxy)phenylboric acid; With potassium carbonate; In ethanol; water; toluene; for 1h;

tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; toluene; for 6h; Heating / reflux;

Reference yield:

: 742100-85-2
tert-butyl (2E)-3-[2-[3-(acetoxymethyl)pyrrolidin-1-yl)-5-[4-(2-butoxyethoxy)phenyl]pyridin-3-yl]-2-methylacrylate

: (2E)-3-[2-[3-(acetoxymethyl)pyrrolidin-1-yl]-5-[4-(2-butoxyethoxy)phenyl]pyridin-3-yl]-2-methylacrylic acid

Guidance literature:: tert-butyl (2E)-3-[2-[3-(acetoxymethyl)pyrrolidin-1-yl)-5-[4-(2-butoxyethoxy)phenyl]pyridin-3-yl]-2-methylacrylate; With hydrogenchloride; In ethyl acetate;

With potassium carbonate; In water; ethyl acetate; at 0 ℃;