(1'S,2S,3R,4R)-3-<(4-tert-Butylphenyl)amino>-4-<(camphanoyloxy)methyl>tetrahydro-2-phenylfuran

Base Information

Chemical Name:(1'S,2S,3R,4R)-3-<(4-tert-Butylphenyl)amino>-4-<(camphanoyloxy)methyl>tetrahydro-2-phenylfuran
CAS No.:134180-73-7
Molecular Formula:C₃₁H₃₉NO₅
Molecular Weight:505.654
Hs Code.:

Synonyms:(1'S,2S,3R,4R)-3-<(4-tert-Butylphenyl)amino>-4-<(camphanoyloxy)methyl>tetrahydro-2-phenylfuran

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Chemical Property of (1'S,2S,3R,4R)-3-<(4-tert-Butylphenyl)amino>-4-<(camphanoyloxy)methyl>tetrahydro-2-phenylfuran

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Technology Process of (1'S,2S,3R,4R)-3-<(4-tert-Butylphenyl)amino>-4-<(camphanoyloxy)methyl>tetrahydro-2-phenylfuran

There total 11 articles about (1'S,2S,3R,4R)-3-<(4-tert-Butylphenyl)amino>-4-<(camphanoyloxy)methyl>tetrahydro-2-phenylfuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 39637-74-6
(1S)-(-)-camphanic chloride

: 134180-69-1
(2S,3R,4R)-3-<(4-tert-Butylphenyl)amino>tetrahydro-4-(hydroxymethyl)-2-phenylfuran

: 134180-73-7
(1'S,2S,3R,4R)-3-<(4-tert-Butylphenyl)amino>-4-<(camphanoyloxy)methyl>tetrahydro-2-phenylfuran

Guidance literature:: With pyridine; dmap; 1a) 0 deg C, 2 h, r. t., 18 h;

Reference yield:

: 13252-73-8
N-(4-tert-Butylphenyl)hydroxylamine

: 134180-73-7
(1'S,2S,3R,4R)-3-<(4-tert-Butylphenyl)amino>-4-<(camphanoyloxy)methyl>tetrahydro-2-phenylfuran

Guidance literature:: Multi-step reaction with 3 steps

1: MgSO₄ / diethyl ether / 1a) 0 deg C, 2 h, b) r. t., 18 h

2: 99 percent / active Raney-nickel / propan-2-ol / Ambient temperature

3: 95 percent / Pyridin / 4-(Dimethylamino)pyridin / 1a) 0 deg C, 2 h, r. t., 18 h

With pyridine; magnesium sulfate; dmap; nickel; In diethyl ether; isopropyl alcohol;

Reference yield:

: 134236-95-6
rac-2-Phenyl-3-oxa-5-hexensaeure-ethylester

: 134180-73-7
(1'S,2S,3R,4R)-3-<(4-tert-Butylphenyl)amino>-4-<(camphanoyloxy)methyl>tetrahydro-2-phenylfuran

Guidance literature:: Multi-step reaction with 4 steps

1: diisobutylaluminum hydride / diethyl ether; hexane / 1 h / -78 °C

2: MgSO₄ / diethyl ether / 1a) 0 deg C, 2 h, b) r. t., 18 h

3: 99 percent / active Raney-nickel / propan-2-ol / Ambient temperature

4: pyridine, 4-(dimethylamino)pyridine / 1a) 0 deg C, 2 h, r. t., 18 h

With pyridine; dmap; diisobutylaluminium hydride; magnesium sulfate; nickel; In diethyl ether; hexane; isopropyl alcohol;