2-(4-chloro-6-(3,4,5-trimethoxyphenylamino)-1,3,5-triazin-2-ylamino)-N-isopropylbenzamide

Base Information

Chemical Name:2-(4-chloro-6-(3,4,5-trimethoxyphenylamino)-1,3,5-triazin-2-ylamino)-N-isopropylbenzamide
CAS No.:1448791-11-4
Molecular Formula:C₂₂H₂₅ClN₆O₄
Molecular Weight:472.931
Hs Code.:

Synonyms:2-(4-chloro-6-(3,4,5-trimethoxyphenylamino)-1,3,5-triazin-2-ylamino)-N-isopropylbenzamide

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Chemical Property of 2-(4-chloro-6-(3,4,5-trimethoxyphenylamino)-1,3,5-triazin-2-ylamino)-N-isopropylbenzamide

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Technology Process of 2-(4-chloro-6-(3,4,5-trimethoxyphenylamino)-1,3,5-triazin-2-ylamino)-N-isopropylbenzamide

There total 2 articles about 2-(4-chloro-6-(3,4,5-trimethoxyphenylamino)-1,3,5-triazin-2-ylamino)-N-isopropylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1393099-43-8
C₁₂H₁₂Cl₂N₄O₃

: 30391-89-0
2-amino-N-isopropylbenzamide

: 1448791-11-4
2-(4-chloro-6-(3,4,5-trimethoxyphenylamino)-1,3,5-triazin-2-ylamino)-N-isopropylbenzamide

Guidance literature:: In tetrahydrofuran; at 20 ℃;
DOI:10.1016/j.bmcl.2013.06.038

Reference yield:

: 24313-88-0
3,4,5-Trimethoxyaniline

: 1448791-11-4
2-(4-chloro-6-(3,4,5-trimethoxyphenylamino)-1,3,5-triazin-2-ylamino)-N-isopropylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / -10 °C

2: tetrahydrofuran / 20 °C

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2013.06.038

Reference yield: 85.0%

: 1448791-11-4
2-(4-chloro-6-(3,4,5-trimethoxyphenylamino)-1,3,5-triazin-2-ylamino)-N-isopropylbenzamide

: 1448791-30-7
N-isopropyl-2-(4-(3,4,5-trimethoxyphenylamino)-1,3,5-triazin-2-ylamino)benzamide

Guidance literature:: With palladium 10% on activated carbon; hydrogen; triethylamine; In tetrahydrofuran; methanol; Inert atmosphere;
DOI:10.1016/j.bmcl.2013.06.038