4,6-dimethyl-2-phenyl-2,3-dihydro-1H-[1,3,2]diazaborolo[4,5-d]pyrimidine-5,7(4H,6H)-dione

Base Information

Chemical Name:4,6-dimethyl-2-phenyl-2,3-dihydro-1H-[1,3,2]diazaborolo[4,5-d]pyrimidine-5,7(4H,6H)-dione
CAS No.:14320-99-1
Molecular Formula:C12H13 B N4 O2
Molecular Weight:256.0682
Hs Code.:
Mol file:14320-99-1.mol

Synonyms:5H-1,3,2-Diazaborolo[4,5-d]pyrimidine-5,7(6H)-dione,1,2,3,4-tetrahydro-4,6-dimethyl-2-phenyl- (6CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,6-dimethyl-2-phenyl-2,3-dihydro-1H-[1,3,2]diazaborolo[4,5-d]pyrimidine-5,7(4H,6H)-dione

Chemical Property:

Vapor Pressure:3.92E-05mmHg at 25°C
Boiling Point:352.1°C at 760 mmHg
Flash Point:166.8°C
Density:1.35g/cm³

Purity/Quality:

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MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4,6-dimethyl-2-phenyl-2,3-dihydro-1H-[1,3,2]diazaborolo[4,5-d]pyrimidine-5,7(4H,6H)-dione

There total 3 articles about 4,6-dimethyl-2-phenyl-2,3-dihydro-1H-[1,3,2]diazaborolo[4,5-d]pyrimidine-5,7(4H,6H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 5440-00-6
4,5-Diamino-1,3-dimethyluracil

: 98-80-6
phenylboronic acid

: 14320-99-1
4,6-dimethyl-2-phenyl-1,2,3,4-tetrahydro-[1,3,2]diazaborolo[4,5-d]pyrimidine-5,7-dione

Guidance literature:: In xylene; byproducts: H2O; distg. the water with the solvent; filtering;
DOI:10.1021/jo01037a021 DOI:10.1021/ja01520a024 DOI:10.1007/BF00631386