tert-butyl trimethylsilyl (4-{1-[(trimethylsilyl)-oxy]-vinyl}-phenyl) carbamate

Base Information

• Chemical Name: tert-butyl trimethylsilyl (4-{1-[(trimethylsilyl)-oxy]-vinyl}-phenyl) carbamate
• CAS No.: 524071-94-1
• Molecular Formula: C₁₉H₃₃NO₃Si₂
• Molecular Weight: 379.647

Synonyms:tert-butyl trimethylsilyl (4-{1-[(trimethylsilyl)-oxy]-vinyl}-phenyl) carbamate

Chemical Property of tert-butyl trimethylsilyl (4-{1-[(trimethylsilyl)-oxy]-vinyl}-phenyl) carbamate

Chemical Property:

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Technology Process of tert-butyl trimethylsilyl (4-{1-[(trimethylsilyl)-oxy]-vinyl}-phenyl) carbamate

There total 1 articles about tert-butyl trimethylsilyl (4-{1-[(trimethylsilyl)-oxy]-vinyl}-phenyl) carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trimethylsilyl trifluoromethanesulfonate (27607-77-8) + tert-butyl 4-acetylphenylcarbamate (232597-42-1) → tert-butyl trimethylsilyl (4-{1-[(trimethylsilyl)-oxy]-vinyl}-phenyl) carbamate (524071-94-1)

Guidance literature:

With triethylamine; In dichloromethane; at -15 - -10 ℃; for 1.5h;

Reference yield:

tert-butyl trimethylsilyl (4-{1-[(trimethylsilyl)-oxy]-vinyl}-phenyl) carbamate (524071-94-1) + (3R,4R)-3-[(R)-1-(tert-butyldimethylsilyloxy)ethyl]-4-acetoxyazetidin-2-one (76899-07-5,78963-47-0,78963-48-1,78963-60-7,80951-41-3,81275-02-7,85647-75-2,85954-95-6,92217-74-8,104527-11-9,76855-69-1) → tert-butyl 4-{[(2R,3S)-3-{(1R)-1-{[tert-butyl-(dimethyl)-silyl]-oxy}-ethyl}-4-oxoazetidin-2-yl]-acetyl}-phenyl carbamate (524071-95-2)

Guidance literature:

With zinc(II) iodide; In dichloromethane; at 20 ℃; for 4h;

upstream raw materials:

trimethylsilyl trifluoromethanesulfonate

tert-butyl 4-acetylphenylcarbamate

Downstream raw materials:

tert-butyl 4-{[(2R,3S)-3-{(1R)-1-{[tert-butyl-(dimethyl)-silyl]-oxy}-ethyl}-4-oxoazetidin-2-yl]-acetyl}-phenyl carbamate

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