2,4,6(1H,3H,5H)-Pyrimidinetrione,1-methyl-5-phenyl-5-propyl-, (5S)-

Base Information

Chemical Name:2,4,6(1H,3H,5H)-Pyrimidinetrione,1-methyl-5-phenyl-5-propyl-, (5S)-
CAS No.:37120-84-6
Molecular Formula:C14H16 N2 O3
Molecular Weight:260.293
Hs Code.:
Mol file:37120-84-6.mol

Synonyms:2,4,6(1H,3H,5H)-Pyrimidinetrione,1-methyl-5-phenyl-5-propyl-, (S)-; (+)-1-Methyl-5-phenyl-5-n-propylbarbituricacid; (+)-1-Methyl-5-phenyl-5-propylbarbituric acid;S-(+)-1-Methyl-5-phenyl-5-propylbarbituric acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,4,6(1H,3H,5H)-Pyrimidinetrione,1-methyl-5-phenyl-5-propyl-, (5S)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,4,6(1H,3H,5H)-Pyrimidinetrione,1-methyl-5-phenyl-5-propyl-, (5S)-

There total 2 articles about 2,4,6(1H,3H,5H)-Pyrimidinetrione,1-methyl-5-phenyl-5-propyl-, (5S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Propionic acid (R)-3-methyl-2,4,6-trioxo-5-phenyl-5-propyl-tetrahydro-pyrimidin-1-ylmethyl ester

: 37120-84-6
(+)-(S)-1-Methyl-5-phenyl-5-propylbarbitursaeure

Guidance literature:: With water; potassium carbonate; In methanol; Yield given;
DOI:10.1016/S0040-4039(00)93597-4

Reference yield:

: 138548-30-8
1,3-bis(propionyloxymethyl)-5-phenyl-5-propylbarbital

: 37120-84-6
(+)-(S)-1-Methyl-5-phenyl-5-propylbarbitursaeure

Guidance literature:: Multi-step reaction with 3 steps

1: H₂O / diisopropyl ether / 9 h / 20 °C / lipase CE

2: (i-Pr)2NEt / CH₂Cl₂

3: K₂CO₃, H₂O / methanol

With water; potassium carbonate; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; di-isopropyl ether;
DOI:10.1016/S0040-4039(00)93597-4