C₂₆H₃₇ClO₃Si₂

Base Information

• Chemical Name: C₂₆H₃₇ClO₃Si₂
• CAS No.: 1163750-71-7
• Molecular Formula: C₂₆H₃₇ClO₃Si₂
• Molecular Weight: 489.202
• Mol file: 1163750-71-7.mol

Synonyms:C₂₆H₃₇ClO₃Si₂

Chemical Property of C₂₆H₃₇ClO₃Si₂

Chemical Property:

Purity/Quality:

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Technology Process of C₂₆H₃₇ClO₃Si₂

There total 2 articles about C₂₆H₃₇ClO₃Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

C26H35ClO3Si2 (1163750-68-2) → C26H37ClO3Si2 (1163750-71-7) + C26H37ClO3Si2

Guidance literature:

With diisobutylaluminium hydride; In toluene; at -78 ℃; for 0.5h; optical yield given as %de; stereoselective reaction; Inert atmosphere;

DOI:10.1002/anie.200900264

Reference yield:

cis-1,2-Dichloroethylene (156-59-2,43695-79-0) + C24H36O3Si2 (1163750-67-1) → C26H37ClO3Si2 (1163750-71-7) + C26H37ClO3Si2

Guidance literature:

cis-1,2-Dichloroethylene; With methyllithium; In diethyl ether; at 0 ℃; Inert atmosphere;

C₂₄H₃₆O₃Si₂; In diethyl ether; at 0 ℃; for 0.166667h; optical yield given as %de; Inert atmosphere;

DOI:10.1021/ja1048994

Reference yield: 99.0%

C26H37ClO3Si2 (1163750-71-7) → C23H29ClO3Si (1163750-74-0)

Guidance literature:

C₂₆H₃₇ClO₃Si₂; With potassium carbonate; In methanol; at 25 ℃; for 1h; Inert atmosphere;

With water; ammonium chloride; In methanol;

DOI:10.1002/anie.200900264

upstream raw materials:

C₂₆H₃₅ClO₃Si₂

cis-1,2-Dichloroethylene

C₂₄H₃₆O₃Si₂

Downstream raw materials:

C₂₃H₂₉ClO₃Si