N-(2,6-dimethyl-4-pentyloxyphenyl)-2-(1-ethoxyethoxy)-4-hydroxy-3,3-dimethylbutyramide

Base Information

Chemical Name:N-(2,6-dimethyl-4-pentyloxyphenyl)-2-(1-ethoxyethoxy)-4-hydroxy-3,3-dimethylbutyramide
CAS No.:616236-26-1
Molecular Formula:C₂₃H₃₉NO₅
Molecular Weight:409.566
Hs Code.:

Synonyms:N-(2,6-dimethyl-4-pentyloxyphenyl)-2-(1-ethoxyethoxy)-4-hydroxy-3,3-dimethylbutyramide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2,6-dimethyl-4-pentyloxyphenyl)-2-(1-ethoxyethoxy)-4-hydroxy-3,3-dimethylbutyramide

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Technology Process of N-(2,6-dimethyl-4-pentyloxyphenyl)-2-(1-ethoxyethoxy)-4-hydroxy-3,3-dimethylbutyramide

There total 3 articles about N-(2,6-dimethyl-4-pentyloxyphenyl)-2-(1-ethoxyethoxy)-4-hydroxy-3,3-dimethylbutyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 3-(1-ethoxy-ethoxy)-4,4-dimethyl-dihydro-furan-2-one

: 616236-25-0
2,6-dimethyl-4-pentyloxyphenylamine

: 616236-26-1
N-(2,6-dimethyl-4-pentyloxyphenyl)-2-(1-ethoxyethoxy)-4-hydroxy-3,3-dimethylbutyramide

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1080/00397910500377545

Reference yield:

: (2,6-dimethyl-4-pentyloxyphenyl)-(4-nitrophenyl)diazene

: 616236-26-1
N-(2,6-dimethyl-4-pentyloxyphenyl)-2-(1-ethoxyethoxy)-4-hydroxy-3,3-dimethylbutyramide

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / sodium dithionite / ethanol; H₂O / 1 h / Heating

2: 58 percent / NaH / dimethylformamide

With sodium dithionite; sodium hydride; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1080/00397910500377545

Reference yield:

: 616236-33-0
1,3-dimethyl-5-(pentyloxy)benzene

: 616236-26-1
N-(2,6-dimethyl-4-pentyloxyphenyl)-2-(1-ethoxyethoxy)-4-hydroxy-3,3-dimethylbutyramide

Guidance literature:: Multi-step reaction with 3 steps

1.1: HCl; NaNO₂ / H₂O / cooling

1.2: 65 percent / AcOH / H₂O / cooling

2.1: 80 percent / sodium dithionite / ethanol; H₂O / 1 h / Heating

3.1: 58 percent / NaH / dimethylformamide

With hydrogenchloride; sodium dithionite; sodium hydride; sodium nitrite; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1080/00397910500377545