Technology Process of C19H27NO4
There total 5 articles about C19H27NO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine hydrofluoride;
In
tetrahydrofuran;
at 20 - 50 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 0.75 h / 130 °C
2.1: dmap; triethylamine; 2,4,6-trichlorobenzoyl chloride / dichloromethane / 14 h / 10 - 20 °C / Cooling with ice
3.1: lithium hexamethyldisilazane / tetrahydrofuran / -50 - 0 °C / Inert atmosphere
3.2: 1 h / 0 - 20 °C
4.1: pyridine hydrofluoride / tetrahydrofuran / 1 h / 20 - 50 °C
With
dmap; pyridine hydrofluoride; 2,4,6-trichlorobenzoyl chloride; triethylamine; lithium hexamethyldisilazane;
In
tetrahydrofuran; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 0.75 h / 130 °C
2.1: dmap; triethylamine; 2,4,6-trichlorobenzoyl chloride / dichloromethane / 14 h / 10 - 20 °C / Cooling with ice
3.1: lithium hexamethyldisilazane / tetrahydrofuran / -50 - 0 °C / Inert atmosphere
3.2: 1 h / 0 - 20 °C
4.1: pyridine hydrofluoride / tetrahydrofuran / 1 h / 20 - 50 °C
With
dmap; pyridine hydrofluoride; 2,4,6-trichlorobenzoyl chloride; triethylamine; lithium hexamethyldisilazane;
In
tetrahydrofuran; dichloromethane;