Technology Process of C38H53NO7Si
There total 5 articles about C38H53NO7Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine;
In
1,2-dichloro-ethane;
at 50 ℃;
for 12h;
Inert atmosphere;
DOI:10.1021/ol103094j
- Guidance literature:
-
Multi-step reaction with 4 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere
2: 1,4-bis-(9-O-dihydroquinidinyl)phthalazine; methanesulfonamide / water; tert-butyl alcohol / 24 h / 20 °C
3: dmap; triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere
4: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 12 h / 50 °C / Inert atmosphere
With
dmap; 1,4-bis-(9-O-dihydroquinidinyl)phthalazine; lithium aluminium tetrahydride; methanesulfonamide; tetra-(n-butyl)ammonium iodide; triethylamine; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane; tert-butyl alcohol;
DOI:10.1021/ol103094j
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dmap; triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere
2: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 12 h / 50 °C / Inert atmosphere
With
dmap; tetra-(n-butyl)ammonium iodide; triethylamine; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ol103094j
