C₂₇H₂₆O₁₄

Base Information

Chemical Name:C₂₇H₂₆O₁₄
CAS No.:1599469-07-4
Molecular Formula:C₂₇H₂₆O₁₄
Molecular Weight:574.495
Hs Code.:

C<sub>27</sub>H<sub>26</sub>O<sub>14</sub>

Synonyms:C₂₇H₂₆O₁₄

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Chemical Property of C₂₇H₂₆O₁₄

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Technology Process of C₂₇H₂₆O₁₄

There total 10 articles about C₂₇H₂₆O₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆₉H₆₂O₁₄

: 1599469-07-4
C₂₇H₂₆O₁₄

: C₂₇H₂₆O₁₄

Guidance literature:: C₆₉H₆₂O₁₄; With palladium 10% on activated carbon; hydrogen; at 20 ℃; under 760.051 Torr;

With 10 wt% Pd(OH)2 on carbon; hydrogen; at 20 ℃; for 2h; under 760.051 Torr; Overall yield = 21 %; Overall yield = 10.8 mg;

Reference yield:

: 1599469-65-4
C₂₄H₂₀O₆

: 1599469-07-4
C₂₇H₂₆O₁₄

: C₂₇H₂₆O₁₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 48 h / 20 °C

2.1: hydrogenchloride / 1,4-dioxane / 0.17 h / 20 °C

3.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / -40 - 20 °C / Inert atmosphere; Molecular sieve

4.1: palladium 10% on activated carbon; hydrogen / 20 °C / 760.05 Torr

4.2: 2 h / 20 °C / 760.05 Torr

With hydrogenchloride; dmap; trimethylsilyl trifluoromethanesulfonate; palladium 10% on activated carbon; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; dichloromethane;

Reference yield:

: 40542-90-3
adipic acid monobenzyl ester

: 1599469-07-4
C₂₇H₂₆O₁₄

: C₂₇H₂₆O₁₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 48 h / 20 °C

2.1: hydrogenchloride / 1,4-dioxane / 0.17 h / 20 °C

3.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / -40 - 20 °C / Inert atmosphere; Molecular sieve

4.1: palladium 10% on activated carbon; hydrogen / 20 °C / 760.05 Torr

4.2: 2 h / 20 °C / 760.05 Torr

With hydrogenchloride; dmap; trimethylsilyl trifluoromethanesulfonate; palladium 10% on activated carbon; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; dichloromethane;