(S)-2-mesityl-5-((2-(4-methoxyphenyl)-1H-pyrrol-1-yl)methyl)-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium chloride

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Chemical Name:(S)-2-mesityl-5-((2-(4-methoxyphenyl)-1H-pyrrol-1-yl)methyl)-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium chloride
CAS No.:1269473-31-5
Molecular Formula:C₂₆H₂₉N₄O*Cl
Molecular Weight:448.995
Hs Code.:

Synonyms:(S)-2-mesityl-5-((2-(4-methoxyphenyl)-1H-pyrrol-1-yl)methyl)-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium chloride

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Chemical Property of (S)-2-mesityl-5-((2-(4-methoxyphenyl)-1H-pyrrol-1-yl)methyl)-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium chloride

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Technology Process of (S)-2-mesityl-5-((2-(4-methoxyphenyl)-1H-pyrrol-1-yl)methyl)-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium chloride

There total 8 articles about (S)-2-mesityl-5-((2-(4-methoxyphenyl)-1H-pyrrol-1-yl)methyl)-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1269473-12-2
(S)-5-(aminomethyl)-2-mesityl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium chloride

: 56139-60-7
1-(4-Methoxyphenyl)-1,4-butandion

: 1269473-31-5
(S)-2-mesityl-5-((2-(4-methoxyphenyl)-1H-pyrrol-1-yl)methyl)-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium chloride

Guidance literature:: With acetic acid; In methanol; at 50 ℃; Inert atmosphere;
DOI:10.1002/asia.201000617

Reference yield:

: 17342-08-4
(S)-Pyroglutaminol

: 1269473-31-5
(S)-2-mesityl-5-((2-(4-methoxyphenyl)-1H-pyrrol-1-yl)methyl)-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium chloride

Guidance literature:: Multi-step reaction with 7 steps

1: triethylamine / 0 °C

2: sodium azide / N,N-dimethyl-formamide / 80 °C

3: dichloromethane / 17 h / 23 °C / Inert atmosphere

4: methanol / 2 h / 50 °C

5: hydrogenchloride; chlorobenzene / 1,4-dioxane / 0.83 h / 100 °C / Inert atmosphere

6: ammonium chloride; zinc / ethanol; water / 1 h / 20 °C

7: acetic acid / methanol / 50 °C / Inert atmosphere

With hydrogenchloride; sodium azide; ammonium chloride; acetic acid; triethylamine; chlorobenzene; zinc; In 1,4-dioxane; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; 7: Paal-Knorr pyrrole synthesis;
DOI:10.1002/asia.201000617

Reference yield:

: 1269473-11-1
(S)-5-(azidomethyl)-2-mesityl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium chloride

: 1269473-31-5
(S)-2-mesityl-5-((2-(4-methoxyphenyl)-1H-pyrrol-1-yl)methyl)-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium chloride; zinc / ethanol; water / 1 h / 20 °C

2: acetic acid / methanol / 50 °C / Inert atmosphere

With ammonium chloride; acetic acid; zinc; In methanol; ethanol; water; 2: Paal-Knorr pyrrole synthesis;
DOI:10.1002/asia.201000617