ethyl N--DL-α-methyltryptophanyl>-N-(2-phenylethyl)-3-aminopropionate

Base Information

Chemical Name:ethyl N--DL-α-methyltryptophanyl>-N-(2-phenylethyl)-3-aminopropionate
CAS No.:150871-33-3
Molecular Formula:C₃₆H₄₅N₃O₅
Molecular Weight:599.77
Hs Code.:

ethyl N-<N-<(2-adamantyloxy)carbonyl>-DL-α-methyltryptophanyl>-N-(2-phenylethyl)-3-aminopropionate

Synonyms:ethyl N--DL-α-methyltryptophanyl>-N-(2-phenylethyl)-3-aminopropionate

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Chemical Property of ethyl N--DL-α-methyltryptophanyl>-N-(2-phenylethyl)-3-aminopropionate

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Technology Process of ethyl N--DL-α-methyltryptophanyl>-N-(2-phenylethyl)-3-aminopropionate

There total 4 articles about ethyl N--DL-α-methyltryptophanyl>-N-(2-phenylethyl)-3-aminopropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 150871-31-1
N-<(2-adamantyloxy)carbonyl>-DL-α-methyltryptophan methyl ester

: 150871-33-3
ethyl N--DL-α-methyltryptophanyl>-N-(2-phenylethyl)-3-aminopropionate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / aq. LiOH / dioxane; ethanol / Ambient temperature

2: 1.) BOP, DIEA / 1.) DMF, RT, 45 min, 2.) DMF, RT, 7 d

With lithium hydroxide; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; ethanol;
DOI:10.1021/jm00072a005

Reference yield:

: 539-74-2
Ethyl 3-bromopropionate

: 150871-33-3
ethyl N--DL-α-methyltryptophanyl>-N-(2-phenylethyl)-3-aminopropionate

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent

2: 1.) BOP, DIEA / 1.) DMF, RT, 45 min, 2.) DMF, RT, 7 d

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
DOI:10.1021/jm00072a005

Reference yield:

: 64-04-0
phenethylamine

: 150871-33-3
ethyl N--DL-α-methyltryptophanyl>-N-(2-phenylethyl)-3-aminopropionate

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent

2: 1.) BOP, DIEA / 1.) DMF, RT, 45 min, 2.) DMF, RT, 7 d

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
DOI:10.1021/jm00072a005