1-(4-chlorophenyl)-2-(1H-imidazol-1-yl)ethyl (2,6-dichloropyridin-4-yl)carbamate

Base Information

Chemical Name:1-(4-chlorophenyl)-2-(1H-imidazol-1-yl)ethyl (2,6-dichloropyridin-4-yl)carbamate
CAS No.:1363792-20-4
Molecular Formula:C₁₇H₁₃Cl₃N₄O₂
Molecular Weight:411.675
Hs Code.:

Synonyms:1-(4-chlorophenyl)-2-(1H-imidazol-1-yl)ethyl (2,6-dichloropyridin-4-yl)carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-chlorophenyl)-2-(1H-imidazol-1-yl)ethyl (2,6-dichloropyridin-4-yl)carbamate

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Technology Process of 1-(4-chlorophenyl)-2-(1H-imidazol-1-yl)ethyl (2,6-dichloropyridin-4-yl)carbamate

There total 3 articles about 1-(4-chlorophenyl)-2-(1H-imidazol-1-yl)ethyl (2,6-dichloropyridin-4-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 178172-70-8,178172-71-9,24155-45-1
(±)-1-(4-chlorophenyl)-2-(1H-imidazol-1-yl)ethanol

: 159178-03-7
2,6-dichloro-4-isocyanatopyridine

: 1363792-20-4
1-(4-chlorophenyl)-2-(1H-imidazol-1-yl)ethyl (2,6-dichloropyridin-4-yl)carbamate

Guidance literature:: In benzene; at 20 ℃; for 48h;
DOI:10.1016/j.ejmech.2012.01.034

Reference yield:

: 2587-02-2
2,6-dichloro-[4]pyridylamine

: 1363792-20-4
1-(4-chlorophenyl)-2-(1H-imidazol-1-yl)ethyl (2,6-dichloropyridin-4-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / benzene / 12 h / 20 °C

2: benzene / 48 h / 20 °C

With triethylamine; In benzene;
DOI:10.1016/j.ejmech.2012.01.034

Reference yield:

: 536-38-9
4-chlorobenzoylmethyl bromide

: 1363792-20-4
1-(4-chlorophenyl)-2-(1H-imidazol-1-yl)ethyl (2,6-dichloropyridin-4-yl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide

2: sodium tetrahydroborate / methanol

3: benzene / 48 h / 20 °C

With sodium tetrahydroborate; In methanol; N,N-dimethyl-formamide; benzene;
DOI:10.1016/j.ejmech.2012.01.034