(3aR,4R,5R,6S,6aR)-4-benzoyloxy-5,6-dibenzyloxyhexahydro-cyclopenta[c]isoxasole

Base Information

Chemical Name:(3aR,4R,5R,6S,6aR)-4-benzoyloxy-5,6-dibenzyloxyhexahydro-cyclopenta[c]isoxasole
CAS No.:219586-98-8
Molecular Formula:C₂₇H₂₇NO₅
Molecular Weight:445.515
Hs Code.:

Synonyms:(3aR,4R,5R,6S,6aR)-4-benzoyloxy-5,6-dibenzyloxyhexahydro-cyclopenta[c]isoxasole

Suppliers and Price of (3aR,4R,5R,6S,6aR)-4-benzoyloxy-5,6-dibenzyloxyhexahydro-cyclopenta[c]isoxasole

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Chemical Property of (3aR,4R,5R,6S,6aR)-4-benzoyloxy-5,6-dibenzyloxyhexahydro-cyclopenta[c]isoxasole

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Technology Process of (3aR,4R,5R,6S,6aR)-4-benzoyloxy-5,6-dibenzyloxyhexahydro-cyclopenta[c]isoxasole

There total 2 articles about (3aR,4R,5R,6S,6aR)-4-benzoyloxy-5,6-dibenzyloxyhexahydro-cyclopenta[c]isoxasole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: Benzoic acid (R)-1-((1S,2R)-1,2-bis-benzyloxy-2-hydroxymethyleneamino-ethyl)-allyl ester

: 219586-98-8
(3aR,4R,5R,6S,6aR)-4-benzoyloxy-5,6-dibenzyloxyhexahydro-cyclopenta[c]isoxasole

Guidance literature:: In toluene; at 110 ℃;
DOI:10.1055/s-1998-1969

Reference yield: 48.0%

: 4-O-Benzoyl-2,3-di-O-benzyl-5,6-dideoxy-D-xylo-hexa-5-enose oxime

: 219586-98-8
(3aR,4R,5R,6S,6aR)-4-benzoyloxy-5,6-dibenzyloxyhexahydro-cyclopenta[c]isoxasole

Guidance literature:: In toluene; at 120 ℃; for 8h;

Reference yield: 33.0%

: 96-26-4,26776-70-5
dihydroxyacetone

: 219586-98-8
(3aR,4R,5R,6S,6aR)-4-benzoyloxy-5,6-dibenzyloxyhexahydro-cyclopenta[c]isoxasole

: 736969-25-8
(3aR,4R,5R,6S,6aR)-4-benzoyloxy-5,6-dibenzyloxy-1-(1,3-dihydroxyprop-2-yl)-hexahydro-cyclopenta[c]isoxazole

Guidance literature:: dihydroxyacetone; (3aR,4R,5R,6S,6aR)-4-benzoyloxy-5,6-dibenzyloxyhexahydro-cyclopenta[c]isoxasole; With acetic acid; In tetrahydrofuran; methanol; at 70 ℃; for 0.5h;

With sodium cyanoborohydride; In tetrahydrofuran; methanol; at 70 ℃; for 10h;