C₉H₁₁BrO₂

Base Information

Chemical Name:C₉H₁₁BrO₂
CAS No.:1329991-96-9
Molecular Formula:C₉H₁₁BrO₂
Molecular Weight:231.089
Hs Code.:

C<sub>9</sub>H<sub>11</sub>BrO<sub>2</sub>

Synonyms:C₉H₁₁BrO₂

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Chemical Property of C₉H₁₁BrO₂

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Technology Process of C₉H₁₁BrO₂

There total 6 articles about C₉H₁₁BrO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 93710-57-7
(2-bromo-6-methoxyphenyl)acetic acid

: 1329991-96-9
C₉H₁₁BrO₂

Guidance literature:: (2-bromo-6-methoxyphenyl)acetic acid; With sodium tetrahydroborate; In tetrahydrofuran; for 0.25h; Inert atmosphere; Cooling with ice;

With boron trifluoride diethyl etherate; In tetrahydrofuran; at 60 ℃; for 1h; Inert atmosphere;
DOI:10.1021/acs.orglett.8b02406

Reference yield:

: 93710-55-5
2-(2-bromo-6-methoxyphenyl)acetonitrile

: 1329991-96-9
C₉H₁₁BrO₂

Guidance literature:: 2-(2-bromo-6-methoxyphenyl)acetonitrile; With hydrogenchloride; water; In acetic acid; for 3h; Reflux;

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; for 24h;

With water; sodium hydroxide; In tetrahydrofuran;

Reference yield:

: 55289-36-6
3-bromo-2-methylaniline

: 1329991-96-9
C₉H₁₁BrO₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium nitrite; sulfuric acid / water / 0.83 h / 0 - 120 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 20 °C

3.1: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 6 h / Reflux

4.1: dimethyl sulfoxide / 3 h / 20 °C

5.1: hydrogenchloride; water / acetic acid / 3 h / Reflux

5.2: 24 h / 0 - 20 °C

With hydrogenchloride; N-Bromosuccinimide; sulfuric acid; water; potassium carbonate; sodium nitrite; dibenzoyl peroxide; In tetrachloromethane; water; acetic acid; dimethyl sulfoxide; N,N-dimethyl-formamide;