Acetic acid (1S,9S,12S)-3-hydroxy-12-isopropyl-9-methyl-4-(3-phenyl-propionyl)-8-oxa-tricyclo[7.3.1.0^2,7]trideca-2⁽⁷⁾,3,5-trien-5-yl ester

Base Information

• Chemical Name: Acetic acid (1S,9S,12S)-3-hydroxy-12-isopropyl-9-methyl-4-(3-phenyl-propionyl)-8-oxa-tricyclo[7.3.1.0^2,7]trideca-2⁽⁷⁾,3,5-trien-5-yl ester
• CAS No.: 122587-93-3
• Molecular Formula: C₂₇H₃₂O₅
• Molecular Weight: 436.548

Synonyms:Acetic acid (1S,9S,12S)-3-hydroxy-12-isopropyl-9-methyl-4-(3-phenyl-propionyl)-8-oxa-tricyclo[7.3.1.0^2,7]trideca-2⁽⁷⁾,3,5-trien-5-yl ester

Chemical Property of Acetic acid (1S,9S,12S)-3-hydroxy-12-isopropyl-9-methyl-4-(3-phenyl-propionyl)-8-oxa-tricyclo[7.3.1.0^2,7]trideca-2⁽⁷⁾,3,5-trien-5-yl ester

Chemical Property:

Purity/Quality:

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Technology Process of Acetic acid (1S,9S,12S)-3-hydroxy-12-isopropyl-9-methyl-4-(3-phenyl-propionyl)-8-oxa-tricyclo[7.3.1.0^2,7]trideca-2⁽⁷⁾,3,5-trien-5-yl ester

There total 3 articles about Acetic acid (1S,9S,12S)-3-hydroxy-12-isopropyl-9-methyl-4-(3-phenyl-propionyl)-8-oxa-tricyclo[7.3.1.0^2,7]trideca-2⁽⁷⁾,3,5-trien-5-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Acetic acid (1S,9S,12R)-3-hydroxy-12-isopropenyl-9-methyl-4-(3-phenyl-propionyl)-8-oxa-tricyclo[7.3.1.02,7]trideca-2(7),3,5-trien-5-yl ester (122587-91-1) → Acetic acid (1S,9S,12S)-3-hydroxy-12-isopropyl-9-methyl-4-(3-phenyl-propionyl)-8-oxa-tricyclo[7.3.1.02,7]trideca-2(7),3,5-trien-5-yl ester (122587-93-3)

Guidance literature:

With hydrogen; platinum(IV) oxide; In ethanol; Yield given; Ambient temperature;

Reference yield:

rubranine (31653-42-6,31759-29-2,111822-12-9,122046-52-0) → Acetic acid (1S,9S,12S)-3-hydroxy-12-isopropyl-9-methyl-4-(3-phenyl-propionyl)-8-oxa-tricyclo[7.3.1.02,7]trideca-2(7),3,5-trien-5-yl ester (122587-93-3)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂ / 10percent Pd-C / ethyl acetate / Ambient temperature

2: 86 percent / acetic acid / 3 h / Heating

3: H₂ / PtO₂ / ethanol / Ambient temperature

With hydrogen; platinum(IV) oxide; palladium on activated charcoal; In ethanol; acetic acid; ethyl acetate;

Reference yield:

C25H28O4 (122587-90-0) → Acetic acid (1S,9S,12S)-3-hydroxy-12-isopropyl-9-methyl-4-(3-phenyl-propionyl)-8-oxa-tricyclo[7.3.1.02,7]trideca-2(7),3,5-trien-5-yl ester (122587-93-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 86 percent / acetic acid / 3 h / Heating

2: H₂ / PtO₂ / ethanol / Ambient temperature

With hydrogen; platinum(IV) oxide; In ethanol; acetic acid;

upstream raw materials:

Acetic acid (1S,9S,12R)-3-hydroxy-12-isopropenyl-9-methyl-4-(3-phenyl-propionyl)-8-oxa-tricyclo[7.3.1.0^2,7]trideca-2⁽⁷⁾,3,5-trien-5-yl ester

rubranine

C₂₅H₂₈O₄

Downstream raw materials:

1-((1S,9S,12S)-3,5-Dihydroxy-12-isopropyl-9-methyl-8-oxa-tricyclo[7.3.1.0^2,7]trideca-2⁽⁷⁾,3,5-trien-4-yl)-3-phenyl-propan-1-one

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