3-((3S)-benzyloxycarbonylaminobutyrylperoxycarbonyl)-(2S)-tert-butoxycarbonylaminopropionic acid tert-butyl ester

Base Information

Chemical Name:3-((3S)-benzyloxycarbonylaminobutyrylperoxycarbonyl)-(2S)-tert-butoxycarbonylaminopropionic acid tert-butyl ester
CAS No.:956472-94-9
Molecular Formula:C₂₅H₃₆N₂O₁₀
Molecular Weight:524.568
Hs Code.:

Synonyms:3-((3S)-benzyloxycarbonylaminobutyrylperoxycarbonyl)-(2S)-tert-butoxycarbonylaminopropionic acid tert-butyl ester

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Chemical Property of 3-((3S)-benzyloxycarbonylaminobutyrylperoxycarbonyl)-(2S)-tert-butoxycarbonylaminopropionic acid tert-butyl ester

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Technology Process of 3-((3S)-benzyloxycarbonylaminobutyrylperoxycarbonyl)-(2S)-tert-butoxycarbonylaminopropionic acid tert-butyl ester

There total 2 articles about 3-((3S)-benzyloxycarbonylaminobutyrylperoxycarbonyl)-(2S)-tert-butoxycarbonylaminopropionic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₂H₁₅NO₅

: 34582-32-6
N-tert-butoxycarbonyl aspartic acid tert-butyl ester

: 956472-94-9
3-((3S)-benzyloxycarbonylaminobutyrylperoxycarbonyl)-(2S)-tert-butoxycarbonylaminopropionic acid tert-butyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃;
DOI:10.1021/ja0746159

Reference yield:

: C₁₂H₁₅NO₅

: 34582-32-6
N-tert-butoxycarbonyl aspartic acid tert-butyl ester

: 956472-94-9
3-((3S)-benzyloxycarbonylaminobutyrylperoxycarbonyl)-(2S)-tert-butoxycarbonylaminopropionic acid tert-butyl ester

: 956472-87-0
3-((3R)-benzyloxycarbonylaminobutyrylperoxycarbonyl)-(2S)-tert-butoxycarbonylaminopropionic acid tert-butyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; Title compound not separated from byproducts.;
DOI:10.1021/ja0746159

Reference yield: 77.0%

: 956472-94-9
3-((3S)-benzyloxycarbonylaminobutyrylperoxycarbonyl)-(2S)-tert-butoxycarbonylaminopropionic acid tert-butyl ester

: 956472-95-0
(5S)-benzyloxycarbonylamino-(2S)-tert-butoxycarbonylaminohexanoic acid tert-butyl ester

Guidance literature:: 3-((3S)-benzyloxycarbonylaminobutyrylperoxycarbonyl)-(2S)-tert-butoxycarbonylaminopropionic acid tert-butyl ester; for 18h; UV-irradiation;

In dichloromethane; for 3h; Further stages.; UV-irradiation;
DOI:10.1021/ja0746159