C₃₈H₅₆O₁₅

Base Information

Chemical Name:C₃₈H₅₆O₁₅
CAS No.:1449432-44-3
Molecular Formula:C₃₈H₅₆O₁₅
Molecular Weight:752.854
Hs Code.:

C<sub>38</sub>H<sub>56</sub>O<sub>15</sub>

Synonyms:C₃₈H₅₆O₁₅

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Chemical Property of C₃₈H₅₆O₁₅

Chemical Property:

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Technology Process of C₃₈H₅₆O₁₅

There total 16 articles about C₃₈H₅₆O₁₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1449432-43-2
C₆₄H₁₁₆O₁₆Si₄

: 1449432-44-3
C₃₈H₅₆O₁₅

Guidance literature:: With dichloro bis(acetonitrile) palladium(II); In water; acetone; at 40 - 45 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.tet.2013.06.105

Reference yield:

: 1449432-35-2
(2S)-2-[(3aS,5S,7aS)-5-[(1,1-Dimethylethyl)dimethylsilyl]oxyhexahydro-7a-methyl-(3H)-inden-1-yl]propan-1-al

: 1449432-44-3
C₃₈H₅₆O₁₅

Guidance literature:: Multi-step reaction with 9 steps

1.1: tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

2.1: dipyridinium dichromate / dichloromethane / 19 h / 20 °C / Inert atmosphere; Molecular sieve

3.1: toluene-4-sulfonic acid; orthoformic acid triethyl ester / dichloromethane / 64 h / 20 °C / Inert atmosphere

4.1: 2,6-dimethylpyridine / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

5.1: osmium(VIII) oxide; pyridine / diethyl ether / 3 h / 20 °C / Inert atmosphere

5.2: Inert atmosphere

6.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

6.2: -78 - 20 °C / Inert atmosphere

7.1: sodium tetrahydroborate; cerium(III) chloride monohydrate / tetrahydrofuran / 5 h / 0 °C

8.1: dichloromethane / 0.25 h / 20 °C / Inert atmosphere; Molecular sieve

8.2: 0.5 h / -20 °C / Inert atmosphere

9.1: dichloro bis(acetonitrile) palladium(II) / water; acetone / 24 h / 40 - 45 °C / Inert atmosphere

With pyridine; 2,6-dimethylpyridine; dichloro bis(acetonitrile) palladium(II); sodium tetrahydroborate; osmium(VIII) oxide; dipyridinium dichromate; oxalyl dichloride; cerium(III) chloride monohydrate; toluene-4-sulfonic acid; dimethyl sulfoxide; orthoformic acid triethyl ester; In tetrahydrofuran; diethyl ether; dichloromethane; water; acetone; 6.1: |Swern Oxidation / 6.2: |Swern Oxidation;
DOI:10.1016/j.tet.2013.06.105

Reference yield:

: 118141-48-3
(3aR,7aS)-1,2,3a,4,5,6,7,7a-octahydro-7a-methyl<1H>inden-1,5-dione

: 1449432-44-3
C₃₈H₅₆O₁₅

Guidance literature:: Multi-step reaction with 16 steps

1.1: oxalic acid / acetonitrile / 1.5 h / 20 °C / Inert atmosphere

2.1: tetrahydrofuran / 15 h / 20 °C / Inert atmosphere

3.1: toluene-4-sulfonic acid / acetone / 1.5 h / 20 °C / Inert atmosphere

4.1: sodium tetrahydroborate / dichloromethane; methanol / 0.75 h / 0 °C / Inert atmosphere

5.1: 2,6-dimethylpyridine / dichloromethane / 2.5 h / 20 °C / Inert atmosphere

6.1: boron trifluoride diethyl etherate / dichloromethane / 0.33 h / 0 °C / Inert atmosphere

7.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 3.5 h / 20 °C / Inert atmosphere

8.1: tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

9.1: dipyridinium dichromate / dichloromethane / 19 h / 20 °C / Inert atmosphere; Molecular sieve

10.1: toluene-4-sulfonic acid; orthoformic acid triethyl ester / dichloromethane / 64 h / 20 °C / Inert atmosphere

11.1: 2,6-dimethylpyridine / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

12.1: osmium(VIII) oxide; pyridine / diethyl ether / 3 h / 20 °C / Inert atmosphere

12.2: Inert atmosphere

13.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

13.2: -78 - 20 °C / Inert atmosphere

14.1: sodium tetrahydroborate; cerium(III) chloride monohydrate / tetrahydrofuran / 5 h / 0 °C

15.1: dichloromethane / 0.25 h / 20 °C / Inert atmosphere; Molecular sieve

15.2: 0.5 h / -20 °C / Inert atmosphere

16.1: dichloro bis(acetonitrile) palladium(II) / water; acetone / 24 h / 40 - 45 °C / Inert atmosphere

With pyridine; 2,6-dimethylpyridine; dichloro bis(acetonitrile) palladium(II); sodium tetrahydroborate; osmium(VIII) oxide; dipyridinium dichromate; oxalyl dichloride; cerium(III) chloride monohydrate; boron trifluoride diethyl etherate; oxalic acid; toluene-4-sulfonic acid; dimethyl sulfoxide; orthoformic acid triethyl ester; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; dimethyl sulfoxide; acetone; acetonitrile; 2.1: |Wittig Olefination / 13.1: |Swern Oxidation / 13.2: |Swern Oxidation;
DOI:10.1016/j.tet.2013.06.105